alpha-Methylbenzenemethanimine

Base Information

Chemical Name:alpha-Methylbenzenemethanimine
CAS No.:13280-20-1
Molecular Formula:C8H9N
Molecular Weight:119.166
Hs Code.:
DSSTox Substance ID:DTXSID801311252
Nikkaji Number:J29.986C

Synonyms:alpha-Methylbenzenemethanimine;acetophenonimine;13280-20-1;SCHEMBL1148180;DTXSID801311252

Suppliers and Price of alpha-Methylbenzenemethanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of alpha-Methylbenzenemethanimine

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:119.073499291
Heavy Atom Count:9
Complexity:101

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=N)C1=CC=CC=C1

Technology Process of alpha-Methylbenzenemethanimine

There total 47 articles about alpha-Methylbenzenemethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 613-91-2
acetophenone oxime

: 13280-20-1
1-phenylethanimine

Guidance literature:: With carbon monoxide; ; In cyclohexane; at 120 ℃; for 12h; under 37503 Torr;
DOI:10.1002/hlca.19910740311

Reference yield:

: 2-azido-1,2-diphenylpropan-1-ol

: 13280-20-1
1-phenylethanimine

: 100-52-7
benzaldehyde

Guidance literature:: With bis[dicarbonylcyclopentadienylruthenium(I)]; In tetrahydrofuran-d8; at 20 ℃; for 6h; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.0c01145

Reference yield:

: 833-81-8
(E)-1,2-diphenylpropene

: 13280-20-1
1-phenylethanimine

: 100-52-7
benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 3-Methylpyrazole; dihydrogen peroxide / water; dichloromethane / 15 h / 20 °C

2: sodium azide; ammonium chloride / ethanol; water / 12 h / 60 °C

3: bis[dicarbonylcyclopentadienylruthenium(I)] / tetrahydrofuran-d8 / 6 h / 20 °C / Inert atmosphere; Irradiation

With sodium azide; 3-Methylpyrazole; bis[dicarbonylcyclopentadienylruthenium(I)]; dihydrogen peroxide; ammonium chloride; In tetrahydrofuran-d8; ethanol; dichloromethane; water;
DOI:10.1021/acs.orglett.0c01145