2,6-diethylpyridine

Base Information

• Chemical Name: 2,6-diethylpyridine
• CAS No.: 935-28-4
• Molecular Formula: C9H13N
• Molecular Weight: 135.209
• Hs Code.: 2933399090
• Mol file: 935-28-4.mol

Synonyms:2,6-Diethylpyridine;

Chemical Property of 2,6-diethylpyridine

Chemical Property:

• Vapor Pressure: 1.46mmHg at 25°C
• Melting Point: 31.33°C (estimate)
• Refractive Index: 1.497
• Boiling Point: 176.6 °C at 760 mmHg
• PKA: 6.56±0.10(Predicted)
• Flash Point: 54.5 °C
• PSA: 12.89000
• Density: 0.911 g/cm³
• LogP: 2.20640
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,6-diethylpyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-diethylpyridine

There total 18 articles about 2,6-diethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,6-Diacetylpyridine (1129-30-2) → 2,6-diethylpyridine (935-28-4)

Guidance literature:

2,6-Diacetylpyridine; With hydrazine; In diethylene glycol; at 170 ℃; for 0.5h;

With potassium hydroxide; In diethylene glycol; at 20 - 200 ℃; for 2h;

Reference yield: 93.0%

2,6-dichloropyridine (2402-78-0) + ethylmagnesium bromide (925-90-6) → 2,6-diethylpyridine (935-28-4)

Guidance literature:

With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In diethyl ether;

DOI:10.1055/s-0029-1219352

Reference yield: 64.0%

α,α'-dihydroxy-1,3-diethylpyridine (143329-89-9) → 2,6-diethylpyridine (935-28-4)

Guidance literature:

With formic acid; zinc; for 24h; Heating;

upstream raw materials:

2,6-dimethylpyridine

methyl iodide

2,6-Diacetylpyridine

dimethyl sulfate

Downstream raw materials:

2,6-diethylpiperidine

2-(1-acetoxy-ethyl)-6-ethyl-pyridine

2-[6-(2-Hydroxy-1-hydroxymethyl-1-methyl-ethyl)-pyridin-2-yl]-2-methyl-propane-1,3-diol

2,6-diethyl-pyridine-1-oxide

Refernces

• 1、 Wu, Junliang,Xu, Kai,Hirao, Hajime,Yoshikai, Naohiko. "Pd-Catalyzed, Ligand-Enabled Stereoselective 1,2-Iodine(III) Shift/1,1-Carboxyalkynylation of Alkynylbenziodoxoles". supporting information. p. 1521 - 1525. Retrieved 2017/02/10.
• 2、 -. "POLYMERIZATION INITIATOR, MODIFIED-CONJUGATED DIENE POLYMER AND TIRE PRODUCED THEREFROM". Page/Page column. . Retrieved 2014/06/24.