Octane, 1-[(trifluoromethyl)thio]-

Base Information

• Chemical Name: Octane, 1-[(trifluoromethyl)thio]-
• CAS No.: 134776-65-1
• Molecular Formula: C9H17F3S
• Molecular Weight: 214.295
• Mol file: 134776-65-1.mol

Synonyms:

Chemical Property of Octane, 1-[(trifluoromethyl)thio]-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Octane, 1-[(trifluoromethyl)thio]-

There total 2 articles about Octane, 1-[(trifluoromethyl)thio]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

octyl thiocyanate (19942-78-0) + (trifluoromethyl)trimethylsilane (81290-20-2) → trimethylsilyl cyanide (7677-24-9) + n-octyll trifluoromethyl sulfide (134776-65-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; 0 deg C, 5 min then rt., 2.5 h;

DOI:10.1016/S0040-4039(96)02216-2

Reference yield:

Bromotrifluoromethane (75-63-8) + Octanethiol (111-88-6) → dioctyl disulfide (822-27-5) + n-octyll trifluoromethyl sulfide (134776-65-1)

Guidance literature:

Octanethiol; With sodium phosphate; In N,N-dimethyl-formamide; for 0.25h;

Bromotrifluoromethane; With rongalite; In N,N-dimethyl-formamide; at 20 ℃; for 8h; under 3375.27 Torr; Title compound not separated from byproducts;

DOI:10.1055/s-2003-37651

upstream raw materials:

octyl thiocyanate

(trifluoromethyl)trimethylsilane

Bromotrifluoromethane

Octanethiol