1-p-Anisyl-3-azetidino>-4-(3,4-methylenedioxyphenyl)azetidin-2-one

Base Information

• Chemical Name: 1-p-Anisyl-3-azetidino>-4-(3,4-methylenedioxyphenyl)azetidin-2-one
• CAS No.: 76640-36-3
• Molecular Formula: C₃₃H₂₆N₂O₈
• Molecular Weight: 578.578

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Chemical Property of 1-p-Anisyl-3-azetidino>-4-(3,4-methylenedioxyphenyl)azetidin-2-one

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Technology Process of 1-p-Anisyl-3-azetidino>-4-(3,4-methylenedioxyphenyl)azetidin-2-one

There total 13 articles about 1-p-Anisyl-3-azetidino>-4-(3,4-methylenedioxyphenyl)azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(3S,4R)-4-Benzo[1,3]dioxol-5-yl-3-{[1-benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-amino}-1-(4-methoxy-phenyl)-azetidin-2-one (76640-39-6) + Phenoxyacetyl chloride (701-99-5) → 1-p-Anisyl-3-azetidino>-4-(3,4-methylenedioxyphenyl)azetidin-2-one (76640-36-3)

Guidance literature:

With triethylamine; In dichloromethane; 1) RT, overnight, 2) reflux, 1h;

Reference yield: 55.0%

N-(benzo[d][1,3]dioxol-5-ylmethylene)-4-methoxyaniline (24033-09-8) + ((2S,3R)-2-Benzo[1,3]dioxol-5-yl-4-oxo-3-phenoxy-azetidin-1-yl)-acetic acid (76640-35-2) → 1-p-Anisyl-3-azetidino>-4-(3,4-methylenedioxyphenyl)azetidin-2-one (76640-36-3)

Guidance literature:

With triethylamine; trichlorophosphate; In dichloromethane; 1) RT, 2) reflux;

Reference yield: 55.0%

3,4-Methylenedioxybenzylidene-p-anisidine (24033-09-8) + ((2S,3R)-2-Benzo[1,3]dioxol-5-yl-4-oxo-3-phenoxy-azetidin-1-yl)-acetic acid (76640-35-2) → 1-p-Anisyl-3-azetidino>-4-(3,4-methylenedioxyphenyl)azetidin-2-one (76640-36-3)

Guidance literature:

With trichlorophosphate;

DOI:10.1016/S0040-4039(00)78671-0

upstream raw materials:

N-(benzo[d][1,3]dioxol-5-ylmethylene)-4-methoxyaniline

((2S,3R)-2-Benzo[1,3]dioxol-5-yl-4-oxo-3-phenoxy-azetidin-1-yl)-acetic acid

3,4-Methylenedioxybenzylidene-p-anisidine

(3S,4R)-4-Benzo[1,3]dioxol-5-yl-3-{[1-benzo[1,3]dioxol-5-yl-meth-(E)-ylidene]-amino}-1-(4-methoxy-phenyl)-azetidin-2-one

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