C₃₇H₃₃BF₂IN₃

Base Information

Chemical Name:C₃₇H₃₃BF₂IN₃
CAS No.:1329012-14-7
Molecular Formula:C₃₇H₃₃BF₂IN₃
Molecular Weight:695.401
Hs Code.:

C<sub>37</sub>H<sub>33</sub>BF<sub>2</sub>IN<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₃₃BF₂IN₃

Chemical Property:

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Technology Process of C₃₇H₃₃BF₂IN₃

There total 10 articles about C₃₇H₃₃BF₂IN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.6%

: 1083009-44-2
2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

: 1310797-90-0
9-butyl-3-ethynyl-9H-carbazole

: 1329012-14-7
C₃₇H₃₃BF₂IN₃

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo200990y

Reference yield:

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 1329012-14-7
C₃₇H₃₃BF₂IN₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 20 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere; Cooling with ice

2.1: N-iodo-succinimide / dichloromethane / 0.5 h / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; copper(l) iodide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; 3.1: Sonogashira coupling;
DOI:10.1021/jo200990y

Reference yield:

: 98-88-4
benzoyl chloride

: 1329012-14-7
C₃₇H₃₃BF₂IN₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 20 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere; Cooling with ice

2.1: N-iodo-succinimide / dichloromethane / 0.5 h / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; N-iodo-succinimide; copper(l) iodide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; 3.1: Sonogashira coupling;
DOI:10.1021/jo200990y