2-(4-methoxyphenyl)fumaronitrile

Base Information Edit

Chemical Name:2-(4-methoxyphenyl)fumaronitrile
CAS No.:110490-04-5
Molecular Formula:C₁₁H₈N₂O
Molecular Weight:184.197
Hs Code.:
Mol file:110490-04-5.mol

Synonyms:

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Chemical Property of 2-(4-methoxyphenyl)fumaronitrile Edit

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Technology Process of 2-(4-methoxyphenyl)fumaronitrile

There total 3 articles about 2-(4-methoxyphenyl)fumaronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7677-24-9
trimethylsilyl cyanide

: 768-60-5
4-methoxyphenylacetylen

: 110490-04-5
2-(4-methoxyphenyl)fumaronitrile

: 110490-05-6
2-(4-methoxyphenyl)maleonitrile

Guidance literature:: With oxygen; palladium dichloride; In toluene; at 20 - 100 ℃; for 17h; optical yield given as %de; stereoselective reaction;
DOI:10.1002/adsc.200900334

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 110490-04-5
2-(4-methoxyphenyl)fumaronitrile

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 4 h / Inert atmosphere; Schlenk technique; Glovebox; Reflux

2: toluene / 80 °C / Inert atmosphere; Schlenk technique; Glovebox

In toluene; acetonitrile;
DOI:10.1021/acs.joc.6b02678