ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate

Base Information

Chemical Name:ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate
CAS No.:1313212-09-7
Molecular Formula:C₁₂H₉FO₅
Molecular Weight:252.199
Hs Code.:

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Chemical Property of ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate

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Technology Process of ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate

There total 1 articles about ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-53-3
diethyl malonate

: 95-01-2
2,4-Dihydroxybenzaldehyde

: 1313212-09-7
ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate

: 1401998-72-8
8-fluoro-3-ethylcarboxylate-7-hydroxycoumarin

: 6093-71-6
7-hydroxy-2-oxo-2H-chromene-3-carboxylic acid ethyl ester

Guidance literature:: 2,4-Dihydroxybenzaldehyde; With Selectfluor; In acetonitrile; at 22 ℃; for 168h; Inert atmosphere; Cooling;

diethyl malonate; With morpholine; acetic acid; In methanol; Inert atmosphere; Cooling; Heating;

Reference yield: 74.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 771-99-3
4-phenylpiperidine

: 1313212-09-7
ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate

: 1421925-03-2
C₂₄H₂₄FNO₅

Guidance literature:: formaldehyd; 4-phenylpiperidine; In acetonitrile; at 65 ℃; for 0.5h;

ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate; In water; acetonitrile; at 85 ℃; for 24h; Darkness;
DOI:10.1002/jccs.201200010

Reference yield: 72.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 92-54-6
4-phenyl-1-piperazine

: 1313212-09-7
ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate

: 1421925-04-3
C₂₃H₂₃FN₂O₅

Guidance literature:: formaldehyd; 4-phenyl-1-piperazine; In acetonitrile; at 65 ℃; for 0.5h;

ethyl 6-fluoro-7-hydroxycoumarin-3-carboxylate; In water; acetonitrile; at 85 ℃; for 24h; Darkness;
DOI:10.1002/jccs.201200010