1-trimethylsiloxy-3-phenylgermatrane

Base Information

Chemical Name:1-trimethylsiloxy-3-phenylgermatrane
CAS No.:594845-01-9
Molecular Formula:C₁₅H₂₅GeNO₄Si
Molecular Weight:384.043
Hs Code.:

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Chemical Property of 1-trimethylsiloxy-3-phenylgermatrane

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Technology Process of 1-trimethylsiloxy-3-phenylgermatrane

There total 2 articles about 1-trimethylsiloxy-3-phenylgermatrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 75-77-4
chloro-trimethyl-silane

: 112987-68-5
1-hydroxy-3-phenylgermatrane

: 594845-01-9
1-trimethylsiloxy-3-phenylgermatrane

Guidance literature:: With triethylamine; In chloroform; byproducts: triethylammonium chloride; (Ar); dropwise addn. of amine and silicon compd. to a suspn. of germanium complex in CHCl3, stirring for 24 h at room temp.; addn. of water, sepn., extn. with CHCl3, washing extract with water, drying (CaCl2), evapn., drying in vac.;
DOI:10.1016/S0022-328X(03)00225-0

Reference yield: 16.0%

: 112987-68-5
1-hydroxy-3-phenylgermatrane

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 594845-01-9
1-trimethylsiloxy-3-phenylgermatrane

Guidance literature:: In xylene; byproducts: NH3; (Ar); refluxing a mixt. of germanium complex and silicon compd. in xylene for 8 h; filtration, cooling filtrate to room temp., filtration, washing with hexane, recrystn. (CH2Cl2/hexane), drying in vac.; elem. anal.;
DOI:10.1016/S0022-328X(03)00225-0

Reference yield: 99.0%

: 594845-01-9
1-trimethylsiloxy-3-phenylgermatrane

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 594845-04-2
[1-(3-phenyl)germatranyl]triflate

Guidance literature:: In xylene; byproducts: ((CH3)3Si)2O; (Ar); dropwise addn. of silicon compd. to a suspn. of germanium complex in xylene at room temp., stirring for 24 h; evapn.; elem. anal.;
DOI:10.1016/S0022-328X(03)00225-0