N,N'-diphenyl-1,1-di-n-butoxysilanediamine

Base Information

• Chemical Name: N,N'-diphenyl-1,1-di-n-butoxysilanediamine
• CAS No.: 18586-46-4
• Molecular Formula: C₂₀H₃₀N₂O₂Si
• Molecular Weight: 358.556
• Mol file: 18586-46-4.mol

Synonyms:

Chemical Property of N,N'-diphenyl-1,1-di-n-butoxysilanediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-diphenyl-1,1-di-n-butoxysilanediamine

There total 1 articles about N,N'-diphenyl-1,1-di-n-butoxysilanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di(n-butoxy)dichlorosilane (18395-82-9) + aniline (62-53-3) → N,N'-diphenyl-1,1-di-n-butoxysilanediamine (18586-46-4)

Guidance literature:

Reference yield:

N,N'-diphenyl-1,1-di-n-butoxysilanediamine (18586-46-4) + titanium tetrachloride (7550-45-0) → N,N'-(phenyl)-1,1-di-n-butoxysilanediamine * 2 titanium (IV) chloride + (C4H9O)Si(NHC6H5)3*2TiCl4

Guidance literature:

In Petroleum ether; addn. of TiCl4 soln. to a soln. of silanediamine, -10°C, equimolar ratios, pptn. of (BuO)Si(NHC6H5)3*2TiCl4, filtration (cold), washing, drying (reduced pressure), filtrate on standing 48 - 72 h, pptn. of (BuO)2Si(NHC6H5)2*2TiCl4; purifn.: filtration (cold), washing, drying (reduced pressure), elem. anal.;

Reference yield:

N,N'-diphenyl-1,1-di-n-butoxysilanediamine (18586-46-4) + tin(IV) chloride (7646-78-8) → N,N'-(phenyl)-1,1-di-n-butoxysilanediamine * 2 tin (IV) chloride + (C4H9O)Si(NHC6H5)3*2SnCl4

Guidance literature:

In Petroleum ether; addn. of SnCl4 soln. to a soln. of silanediamine, -10°C, equimolar ratios, pptn. of (BuO)Si(NHC6H5)3*2SnCl4, filtration (cold), washing, drying (reduced pressure), filtrate on standing 48 - 72 h, pptn. of (BuO)2Si(NHC6H5)2*2SnCl4; purifn.: filtration (cold), washing, drying (reduced pressure), elem. anal.;

upstream raw materials:

di(n-butoxy)dichlorosilane

aniline