C₁₇H₁₄BrN₃O₃

Base Information

Chemical Name:C₁₇H₁₄BrN₃O₃
CAS No.:1428538-82-2
Molecular Formula:C₁₇H₁₄BrN₃O₃
Molecular Weight:388.22
Hs Code.:

C<sub>17</sub>H<sub>14</sub>BrN<sub>3</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₁₇H₁₄BrN₃O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₇H₁₄BrN₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₇H₁₄BrN₃O₃

There total 5 articles about C₁₇H₁₄BrN₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1428538-87-7
4-[3-(4-nitrophenyl)-1H-pyrazol-5-yl]phenol

: 106-93-4
ethylene dibromide

: 1428538-82-2
C₁₇H₁₄BrN₃O₃

Guidance literature:: 4-[3-(4-nitrophenyl)-1H-pyrazol-5-yl]phenol; With tetrabutyl ammonium fluoride; sodium hydroxide; In tetrahydrofuran; ethanol; at 30 ℃; for 0.333333h;

ethylene dibromide; In tetrahydrofuran; ethanol; for 1.5h; Microwave irradiation;
DOI:10.1002/ardp.201200057

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1428538-82-2
C₁₇H₁₄BrN₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 0 °C / Inert atmosphere; Cooling with ice

1.2: Inert atmosphere; Cooling with ice

2.1: acetic acid; hydrazine hydrate / toluene; tetrahydrofuran; N,N-dimethyl-formamide; ethanol / 0.25 h / Inert atmosphere; Reflux

3.1: boron tribromide / dichloromethane / 19 h / -78 - 20 °C

4.1: tetrabutyl ammonium fluoride; sodium hydroxide / tetrahydrofuran; ethanol / 0.33 h / 30 °C

4.2: 1.5 h / Microwave irradiation

With tetrabutyl ammonium fluoride; boron tribromide; hydrazine hydrate; acetic acid; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ardp.201200057

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1428538-82-2
C₁₇H₁₄BrN₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 0 °C / Inert atmosphere; Cooling with ice

1.2: Inert atmosphere; Cooling with ice

2.1: acetic acid; hydrazine hydrate / toluene; tetrahydrofuran; N,N-dimethyl-formamide; ethanol / 0.25 h / Inert atmosphere; Reflux

3.1: boron tribromide / dichloromethane / 19 h / -78 - 20 °C

4.1: tetrabutyl ammonium fluoride; sodium hydroxide / tetrahydrofuran; ethanol / 0.33 h / 30 °C

4.2: 1.5 h / Microwave irradiation

With tetrabutyl ammonium fluoride; boron tribromide; hydrazine hydrate; acetic acid; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/ardp.201200057