Technology Process of 4-Methylamino-1-phenyl-cyclohexancarbonsaeuremethylester
There total 7 articles about 4-Methylamino-1-phenyl-cyclohexancarbonsaeuremethylester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
platinum(IV) oxide;
In
methanol; water;
Ambient temperature;
DOI:10.1002/ardp.19803130603
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 55 percent / p-toluenesulfonic acid / CH2Cl2 / 24 h / Heating
2: 96 percent / NaNH2 / dimethylsulfoxide / 1 h / 50 °C
3: 77 percent / KOH / ethane-1,2-diol; H2O / 48 h / Heating
4: 92 percent / acetic acid / 24 h / Heating
5: 1.) NaOH / 1.) EtOH, HMPT, 10 min, 2.) 50 deg C, 2 h
6: 87 percent / H2 / PtO2 / H2O; methanol / Ambient temperature
With
potassium hydroxide; sodium hydroxide; hydrogen; toluene-4-sulfonic acid; sodium amide; acetic acid;
platinum(IV) oxide;
In
methanol; dichloromethane; water; ethylene glycol; dimethyl sulfoxide;
DOI:10.1002/ardp.19803130603
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 96 percent / NaNH2 / dimethylsulfoxide / 1 h / 50 °C
2: 77 percent / KOH / ethane-1,2-diol; H2O / 48 h / Heating
3: 92 percent / acetic acid / 24 h / Heating
4: 1.) NaOH / 1.) EtOH, HMPT, 10 min, 2.) 50 deg C, 2 h
5: 87 percent / H2 / PtO2 / H2O; methanol / Ambient temperature
With
potassium hydroxide; sodium hydroxide; hydrogen; sodium amide; acetic acid;
platinum(IV) oxide;
In
methanol; water; ethylene glycol; dimethyl sulfoxide;
DOI:10.1002/ardp.19803130603
