[Os(C₅H₅)Cl(PH(C₆H₅)2)(P(CH(CH₃)2)3)]

Base Information

Chemical Name:[Os(C₅H₅)Cl(PH(C₆H₅)2)(P(CH(CH₃)2)3)]
CAS No.:308305-51-3
Molecular Formula:C₂₆H₃₇ClOsP₂
Molecular Weight:637.18
Hs Code.:

[Os(C<sub>5</sub>H<sub>5</sub>)Cl(PH(C<sub>6</sub>H<sub>5</sub>)2)(P(CH(CH<sub>3</sub>)2)3)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Os(C₅H₅)Cl(PH(C₆H₅)2)(P(CH(CH₃)2)3)]

Chemical Property:

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Technology Process of [Os(C₅H₅)Cl(PH(C₆H₅)2)(P(CH(CH₃)2)3)]

There total 1 articles about [Os(C₅H₅)Cl(PH(C₆H₅)2)(P(CH(CH₃)2)3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 196520-48-6
(η(5)-cyclopentadienyl)OsCl(triisopropylphosphine)2

: 829-85-6
diphenylphosphane

: 308305-51-3
[Os(C₅H₅)Cl(PH(C₆H₅)2)(P(CH(CH₃)2)3)]

Guidance literature:: In pentane; byproducts: P(CH(CH3)2)3; Standard Schlenk technique; PHPh2 added to suspn. of Os complex in pentane; mixt. stirred at room temp. for 5 h; partially evapd.; filtered; washed (pentane); dried in vac.; elem. anal.;
DOI:10.1021/om000446o

Reference yield: 95.0%

: 60969-19-9
thallium(I) hexafluorophosphate

: 308305-51-3
[Os(C₅H₅)Cl(PH(C₆H₅)2)(P(CH(CH₃)2)3)]

: 7732-18-5
water

: [OsH₂(C₅H₅)(P(OH)(C₆H₅)2)(P(CH(CH₃)2)3)]⁽¹⁺⁾*PF₆^(1-)=[OsH₂(C₅H₅)(P(OH)(C₆H₅)2)(P(CH(CH₃)2)3)]⁽¹⁺⁾*PF₆^(1-)

Guidance literature:: In water; acetone; byproducts: TlCl; Standard Schlenk technique; TlPF6 added to soln. of Os complex in acetone; mixt. stirred at room temp. for 15 min; filtered through Kieselguhr; solvent removed in vac.; Et2O added; filtered; washed (Et2O); dried in vac.; elem. anal.;
DOI:10.1021/om000446o

Reference yield: 94.0%

: 67-56-1
methanol

: 60969-19-9
thallium(I) hexafluorophosphate

: 308305-51-3
[Os(C₅H₅)Cl(PH(C₆H₅)2)(P(CH(CH₃)2)3)]

: 308305-55-7
[OsH₂(C₅H₅)(P(OCH₃)(C₆H₅)2)(P(CH(CH₃)2)3)]⁽¹⁺⁾*PF₆^(1-)=[OsH₂(C₅H₅)(P(OCH₃)(C₆H₅)2)(P(CH(CH₃)2)3)]⁽¹⁺⁾*PF₆^(1-)

Guidance literature:: In methanol; byproducts: TlCl; Standard Schlenk technique; TlPF6 added to soln. of Os complex in methanol; mixt. stirred at room temp. for 15 min; filtered through Kieselguhr; solvent removed in vac.; Et2O added; filtered; washed (Et2O); dried in vac.; elem. anal.;
DOI:10.1021/om000446o