trimethylamine alane

Base Information

Chemical Name:trimethylamine alane
CAS No.:855944-65-9
Molecular Formula:C₃H₁₂AlN
Molecular Weight:89.1165
Hs Code.:

Synonyms:

Suppliers and Price of trimethylamine alane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimethylamine alane

Chemical Property:

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Technology Process of trimethylamine alane

There total 4 articles about trimethylamine alane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7446-70-0
aluminium trichloride

: sodium aluminum tetrahydride

: 75-50-3
trimethylamine

: 16842-00-5,855944-65-9
trimethylamine alane

Guidance literature:: In diethyl ether; toluene; byproducts: NaCl; AlCl3 in ether was added to suspn. NaAlH4 in toluene-ether in 30 min andstired for 4 h, soln. was filtered and cooled to 0°C, Me3N was a dded; solvent was removed;
DOI:10.1021/ic802262h

Reference yield: 72.0%

: 16853-85-3
lithium aluminium tetrahydride

: 593-81-7
trimethylamine hydrochloride

: 16842-00-5,855944-65-9
trimethylamine alane

Guidance literature:: In diethyl ether; at -50 - 0 ℃; for 4h; Inert atmosphere;
DOI:10.1039/d0dt01820a

Reference yield:

: 7446-70-0,7784-13-6
aluminum (III) chloride

: 16853-85-3
lithium aluminium tetrahydride

: 75-50-3
trimethylamine

: 16842-00-5,855944-65-9
trimethylamine alane

Guidance literature:: aluminum (III) chloride; lithium aluminium tetrahydride; In diethyl ether; at -10 ℃; for 0.00833333h;

trimethylamine; In diethyl ether; at -10 ℃; for 5h; Product distribution / selectivity;