2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide

Base Information

• Chemical Name: 2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide
• CAS No.: 1403612-04-3
• Molecular Formula: C₁₉H₁₆N₂O₃
• Molecular Weight: 320.348
• Mol file: 1403612-04-3.mol

Synonyms:

Chemical Property of 2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide

There total 2 articles about 2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-hydroxy-2-acetonaphthone (711-79-5) + 2-Hydroxybenzoylhydrazine (936-02-7) → 2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide (1403612-04-3)

Guidance literature:

In methanol;

DOI:10.1134/S1070328412070111

Reference yield: 60.0%

1-(2-hydroxy-1-naphthyl)ethan-1-one (574-19-6) + 2-Hydroxybenzoylhydrazine (936-02-7) → 2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide (1403612-04-3)

Guidance literature:

In ethanol;

DOI:10.1021/ic401866x

Reference yield: 80.0%

methanol (67-56-1) + bis(acetylacetonate)oxidovanadium(IV) + 2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide (1403612-04-3) → [oxovanadium(V)(OMe)(2-hydroxy-N'-[1-(2-hydroxynaphthyl)ethylidene]benzohydrazide(-2H))]

Guidance literature:

In methanol; MeOH soln. of C19H16N2O3 added to stirred MeOH soln. of V complex, stirred for 30 min at room temp.; crystd. by slow evapn. for a few d, isolated by filtration; elem. anal.;

DOI:10.1134/S1070328412070111

upstream raw materials:

1-hydroxy-2-acetonaphthone

2-Hydroxybenzoylhydrazine

1-(2-hydroxy-1-naphthyl)ethan-1-one