triphenylantimony di(p-toluenesulfonate)

Base Information

Chemical Name:triphenylantimony di(p-toluenesulfonate)
CAS No.:112134-57-3
Molecular Formula:C₃₂H₂₉O₆S₂Sb
Molecular Weight:695.461
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylantimony di(p-toluenesulfonate)

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Technology Process of triphenylantimony di(p-toluenesulfonate)

There total 3 articles about triphenylantimony di(p-toluenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 102614-53-9
triphenylantimony oxide dimer

: 104-15-4
toluene-4-sulfonic acid

: 112134-57-3
triphenylantimony di(p-toluenesulfonate)

Guidance literature:: In acetone; suspending Me3Sb(OH)2 in a mixt. of acetone and 2,2-dimethoxypropane, adding the sulfonic acid, pptn.; filtering by suction, washing (abs. acetone or ether), drying (desiccator, silica gel); elem. anal.;

Reference yield: 68.0%

: 7722-84-1
dihydrogen peroxide

: 603-36-1
triphenylantimony

: 104-15-4
toluene-4-sulfonic acid

: 112134-57-3
triphenylantimony di(p-toluenesulfonate)

Guidance literature:: In diethyl ether; 20°C, 12 h;

Reference yield: 4.5%

: 603-36-1
triphenylantimony

: 104-15-4
toluene-4-sulfonic acid

: 112134-57-3
triphenylantimony di(p-toluenesulfonate)

: phenylantimony bis(p-toluenesulfonate)

Guidance literature:: In toluene; byproducts: C6H6; refluxing for 1 h; cooling, mixture filtration, solvent removing, residue re-crystn. (benzene-isopropanol);