triphenylantimony di(p-toluenesulfonate)

Base Information

• Chemical Name: triphenylantimony di(p-toluenesulfonate)
• CAS No.: 112134-57-3
• Molecular Formula: C₃₂H₂₉O₆S₂Sb
• Molecular Weight: 695.461
• Mol file: 112134-57-3.mol

Synonyms:

Chemical Property of triphenylantimony di(p-toluenesulfonate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of triphenylantimony di(p-toluenesulfonate)

There total 3 articles about triphenylantimony di(p-toluenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

triphenylantimony oxide dimer (102614-53-9) + toluene-4-sulfonic acid (104-15-4) → triphenylantimony di(p-toluenesulfonate) (112134-57-3)

Guidance literature:

In acetone; suspending Me3Sb(OH)2 in a mixt. of acetone and 2,2-dimethoxypropane, adding the sulfonic acid, pptn.; filtering by suction, washing (abs. acetone or ether), drying (desiccator, silica gel); elem. anal.;

Reference yield: 68.0%

dihydrogen peroxide (7722-84-1) + triphenylantimony (603-36-1) + toluene-4-sulfonic acid (104-15-4) → triphenylantimony di(p-toluenesulfonate) (112134-57-3)

Guidance literature:

In diethyl ether; 20°C, 12 h;

Reference yield: 4.5%

triphenylantimony (603-36-1) + toluene-4-sulfonic acid (104-15-4) → triphenylantimony di(p-toluenesulfonate) (112134-57-3) + phenylantimony bis(p-toluenesulfonate)

Guidance literature:

In toluene; byproducts: C6H6; refluxing for 1 h; cooling, mixture filtration, solvent removing, residue re-crystn. (benzene-isopropanol);

upstream raw materials:

triphenylantimony oxide dimer

toluene-4-sulfonic acid

dihydrogen peroxide

triphenylantimony