[Mo2Cp2(μ-SMe)3(μ-Cl)]

Base Information

Chemical Name:[Mo2Cp2(μ-SMe)3(μ-Cl)]
CAS No.:779340-57-7
Molecular Formula:C₁₃H₁₉ClMo₂S₃
Molecular Weight:498.825
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Mo2Cp2(μ-SMe)3(μ-Cl)]

Chemical Property:

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Technology Process of [Mo2Cp2(μ-SMe)3(μ-Cl)]

There total 1 articles about [Mo2Cp2(μ-SMe)3(μ-Cl)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: tetrafluoroboric acid

: 75-09-2
dichloromethane

: [Mo2(η5-C5H5)2(μ-SMe)3(μ-CHCH2Ph)](1+)

: 779340-57-7,103619-79-0
[Mo2Cp2(μ-SMe)3(μ-Cl)]

: [Mo2(η5-C5H5)2(μ-SH)3(μ-CCH2Ph)]

: [Mo2(η5-C5H5)2(μ-SMe)3(μ-CH2CH2Ph)]

Guidance literature:: In dichloromethane; Electrolysis; (Schlenk); to a soln. of complex in CH2Cl2-tetra-n-butylammonium hexafluorophosphate under N2 was added 1 or 2 equiv of HBF4/diethyl ether, controlled-potential electrolysis was performed at -1.2 V; the catholyte was transferred, the solvent was removed in vac., pentane was added, the mixt. was stirred for 10 min, filtered, dried under vac.,; detected by (1)H NMR spectra;
DOI:10.1021/om050761g

Reference yield: 50.0%

: 779340-57-7,103619-79-0
[Mo2Cp2(μ-SMe)3(μ-Cl)]

: 100-63-0
phenylhydrazine

: 205067-88-5,205067-89-6,434309-23-6
[Mo2Cp2(μ-SMe)3(μ-η(1)-N2Ph)]

: 434309-23-6,205067-88-5,205067-89-6
[Mo2Cp2(μ-SMe)3(μ-η(2)-N2Ph)]

Guidance literature:: In tetrahydrofuran; byproducts: NH4Cl; 70°C (6 h); filtering, evapn., chromy. (SiO2, CH2Cl2 / THF = 9 : 1, THF), washing (pentane); elem. anal.;
DOI:10.1021/om971114v