Benzene, 1-methoxy-3-[(phenylthio)methyl]-

Base Information

Chemical Name:Benzene, 1-methoxy-3-[(phenylthio)methyl]-
CAS No.:139599-68-1
Molecular Formula:C14H14OS
Molecular Weight:230.331
Hs Code.:
DSSTox Substance ID:DTXSID90402256
Nikkaji Number:J768.124K
Mol file:139599-68-1.mol

Synonyms:Benzene, 1-methoxy-3-[(phenylthio)methyl]-;139599-68-1;Phenyl 3-methoxybenzyl sulfide;DTXSID90402256;AKOS024382384

Suppliers and Price of Benzene, 1-methoxy-3-[(phenylthio)methyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-methoxy-3-[(phenylthio)methyl]-

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:230.07653624
Heavy Atom Count:16
Complexity:189

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)CSC2=CC=CC=C2

Technology Process of Benzene, 1-methoxy-3-[(phenylthio)methyl]-

There total 8 articles about Benzene, 1-methoxy-3-[(phenylthio)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 108-98-5
thiophenol

: 874-98-6
1-bromomethyl-3-methoxybenzene

: 139599-68-1
(3-methoxybenzyl)(phenyl)sulfide

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In benzene; for 0.5h;

Reference yield: 52.0%

: 1193-82-4
racemic methyl phenyl sulfoxide

: 36282-40-3
(3-methoxyphenyl)magnesium bromide

: 139599-68-1
(3-methoxybenzyl)(phenyl)sulfide

Guidance literature:: racemic methyl phenyl sulfoxide; With diisopropylaminomagnesium chloride lithium chloride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

(3-methoxyphenyl)magnesium bromide; In tetrahydrofuran; at 0 - 65 ℃; for 14h; Inert atmosphere;
DOI:10.1002/anie.201709715

Reference yield: 44.0%

: 6971-51-3
3-methoxybenzyl alcohol

: 882-33-7
diphenyldisulfane

: 139599-68-1
(3-methoxybenzyl)(phenyl)sulfide

Guidance literature:: With iodine; In 1-methyl-pyrrolidin-2-one; at 130 ℃; for 0.666667h; Sealed tube; Microwave irradiation;
DOI:10.1002/cjoc.201200723