N'-(2-METHOXY-BENZYL)-N,N-DIMETHYL-ETHANE-1,2-DIAMINE

Base Information

• Chemical Name: N'-(2-METHOXY-BENZYL)-N,N-DIMETHYL-ETHANE-1,2-DIAMINE
• CAS No.: 626216-36-2
• Molecular Formula: C₁₂H₂₀N₂O
• Molecular Weight: 208.304
• Mol file: 626216-36-2.mol

Synonyms:

Chemical Property of N'-(2-METHOXY-BENZYL)-N,N-DIMETHYL-ETHANE-1,2-DIAMINE

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

N''-(2-Methoxy-benzyl)-N,N-dimethyl-ethane-1,2-diamine ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of N'-(2-METHOXY-BENZYL)-N,N-DIMETHYL-ETHANE-1,2-DIAMINE

There total 4 articles about N'-(2-METHOXY-BENZYL)-N,N-DIMETHYL-ETHANE-1,2-DIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

OCH3C6H4CHNCH2CH2N(CH3)2 → N'-(2-methoxy-benzyl)-N,N-dimethyl-ethylenediamine (626216-36-2)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c0dt00250j

Reference yield:

ortho-anisaldehyde (135-02-4) → N'-(2-methoxy-benzyl)-N,N-dimethyl-ethylenediamine (626216-36-2)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 24 h / Inert atmosphere; Reflux

2: sodium tetrahydroborate / methanol / 12 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; In methanol;

DOI:10.1039/c0dt00250j

Reference yield:

N,N-dimethylethylenediamine (108-00-9) + ortho-anisaldehyde (135-02-4) → N'-(2-methoxy-benzyl)-N,N-dimethyl-ethylenediamine (626216-36-2)

Guidance literature:

N,N-dimethylethylenediamine; ortho-anisaldehyde; In ethanol; for 12h; Inert atmosphere; Schlenk technique; Reflux;

With sodium tetrahydroborate; In ethanol; for 12h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1039/c4dt01122h

upstream raw materials:

2-methoxybenzylamine

2-(dimethylamino)ethyl chloride

ortho-anisaldehyde

N,N-dimethylethylenediamine

Downstream raw materials:

6-tert-butyl-2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4-methylphenol

4,6-di-tert-butyl-2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)phenol

2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dicumylphenol

2-(N-(2-methoxybenzyl)-N-[2-(N,N-dimethyl)aminoethyl]aminomethyl)-4,6-dichlorophenol