cyclohexylphosphine - borane

Base Information

Chemical Name:cyclohexylphosphine - borane
CAS No.:181864-73-3
Molecular Formula:C₆H₁₆BP
Molecular Weight:129.978
Hs Code.:

Synonyms:

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Chemical Property of cyclohexylphosphine - borane

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Technology Process of cyclohexylphosphine - borane

There total 2 articles about cyclohexylphosphine - borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: borane tetrahydrofuran

: 822-68-4
cyclohexylphosphine

: 181864-73-3
cyclohexylphosphine - borane

Guidance literature:: In tetrahydrofuran; Ar-atmosphere; stirring (-20°C, 2 h); evapn. (room temp.); detd. by NMR spectroscopy;
DOI:10.1021/om9603373

Reference yield:

: 13292-87-0
dimethylsulfide borane complex

: 822-68-4
cyclohexylphosphine

: 181864-73-3
cyclohexylphosphine - borane

Guidance literature:: at 0 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201800742

Reference yield: 40.0%

: 181864-73-3
cyclohexylphosphine - borane

: 107-99-3
2-(dimethylamino)ethyl chloride

: 181864-74-4
[(CH₃)2NC₂H₄]2P(BH₃)C₆H₁₁

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; Ar-atmosphere; stirring (-78°C to room temp., 2 h), amine soln. (THF) addn. (-78°C), -78°C (2 h), stirring (room temp., overnight); evapn., chromy. (SiO2, MeOH); elem. anal.;
DOI:10.1021/om9603373