3-methyl-1-[(1-pyrazolyl)methyl]imidazolium tetraphenylborate

Base Information

Chemical Name:3-methyl-1-[(1-pyrazolyl)methyl]imidazolium tetraphenylborate
CAS No.:911122-40-2
Molecular Formula:C₈H₁₁N₄*C₂₄H₂₀B
Molecular Weight:482.436
Hs Code.:

Synonyms:

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Chemical Property of 3-methyl-1-[(1-pyrazolyl)methyl]imidazolium tetraphenylborate

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Technology Process of 3-methyl-1-[(1-pyrazolyl)methyl]imidazolium tetraphenylborate

There total 2 articles about 3-methyl-1-[(1-pyrazolyl)methyl]imidazolium tetraphenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 616-47-7
1-methyl-1H-imidazole

: 143-66-8
sodium tetraphenyl borate

: 73901-67-4
1-(chloromethyl)pyrazole hydrochloride

: 911122-40-2
3-methyl-1-[(1-pyrazolyl)methyl]imidazolium tetraphenylborate

Guidance literature:: 1-methyl-1H-imidazole; 1-(chloromethyl)pyrazole hydrochloride; In toluene; for 2h; Reflux;

sodium tetraphenyl borate; In toluene; at 20 ℃; for 1.08333h; Reflux;
DOI:10.1039/b906724h

Reference yield:

: 3-methyl-1-(pyrazolylmethyl)imidazolium chloride

: 143-66-8
sodium tetraphenyl borate

: 911122-40-2
3-methyl-1-[(1-pyrazolyl)methyl]imidazolium tetraphenylborate

Guidance literature:: In toluene; for 3h; Heating;
DOI:10.1039/b603455a

Reference yield: 89.0%

: 911122-40-2
3-methyl-1-[(1-pyrazolyl)methyl]imidazolium tetraphenylborate

: 67-56-1
methanol

: 73456-54-9
bis[(1,2,5,6-η)-1,5-cyclooctadiene]di-μ-ethoxo-dirhodium(I)

: [Rh(1,5-cyclooctadiene)(3-methyl-1-[(1-pyrazolyl)methyl]imidazolylidene)][tetraphenylborate]*2methanol

Guidance literature:: With sodium ethoxide; In methanol; (inert atm.); addn. of a suspn. of ligand in methanol to a soln. of metal complex and sodium ethoxide in methanol, stirring for 3 h; filtration, concn. in vac., washing ppt. with hexane, drying in vac.; elem. anal.;
DOI:10.1039/b603455a