9-(cyanoethyl)-9-anilinofluorene

Base Information

• Chemical Name: 9-(cyanoethyl)-9-anilinofluorene
• CAS No.: 79817-29-1
• Molecular Formula: C₂₂H₁₈N₂
• Molecular Weight: 310.398
• Mol file: 79817-29-1.mol

Synonyms:

Chemical Property of 9-(cyanoethyl)-9-anilinofluorene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-(cyanoethyl)-9-anilinofluorene

There total 3 articles about 9-(cyanoethyl)-9-anilinofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

N-phenylfluorenimine (10183-82-1) + 4-Chlorobutanoyl chloride (4635-59-0) → N-phenylcyclopropanecarboxamide (2759-52-6) + N-phenyl-9H-fluoren-9-amine (31859-87-7) + 9-(cyanoethyl)-9-anilinofluorene (79817-29-1) + 9-(cyclopropylcarbonyl)-9-anilinofluorene (79817-36-0)

Guidance literature:

In acetonitrile; at 18 ℃; Further byproducts given; electrochemical reduction: mercury cathode, -1.42 V;

DOI:10.1021/jo00341a029

Reference yield: 16.0%

N-phenylfluorenimine (10183-82-1) + 4-Chlorobutanoyl chloride (4635-59-0) → N-phenyl-9H-fluoren-9-amine (31859-87-7) + 9-(cyanoethyl)-9-anilinofluorene (79817-29-1) + 9-fluorene (79817-39-3) + 9-(cyclopropylcarbonyl)-9-anilinofluorene (79817-36-0)

Guidance literature:

In acetonitrile; at 18 ℃; Further byproducts given; electrochemical reduction: mercury cathode, -1.42 V;

DOI:10.1021/jo00341a029

Reference yield: 16.0%

N-phenylfluorenimine (10183-82-1) + acetonitrile (75-05-8,26809-02-9) + 4-Chlorobutanoyl chloride (4635-59-0) → N-phenylcyclopropanecarboxamide (2759-52-6) + N-phenyl-9H-fluoren-9-amine (31859-87-7) + 9-(cyanoethyl)-9-anilinofluorene (79817-29-1) + 9-(cyclopropylcarbonyl)-9-anilinofluorene (79817-36-0)

Guidance literature:

at 18 ℃; Further byproducts given; elelctrochemical reduction: mercury cathode, -1.42 V;

DOI:10.1021/jo00341a029

upstream raw materials:

N-phenylfluorenimine

acetonitrile

4-Chlorobutanoyl chloride