cis-(1,2-bis(diphenylphosphino)ethane)(2-hydroxypropane-1,3-dithiolato)platinum(II)

Base Information

Chemical Name:cis-(1,2-bis(diphenylphosphino)ethane)(2-hydroxypropane-1,3-dithiolato)platinum(II)
CAS No.:1280725-13-4
Molecular Formula:C₂₉H₃₀OP₂PtS₂
Molecular Weight:715.716
Hs Code.:

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Chemical Property of cis-(1,2-bis(diphenylphosphino)ethane)(2-hydroxypropane-1,3-dithiolato)platinum(II)

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Technology Process of cis-(1,2-bis(diphenylphosphino)ethane)(2-hydroxypropane-1,3-dithiolato)platinum(II)

There total 2 articles about cis-(1,2-bis(diphenylphosphino)ethane)(2-hydroxypropane-1,3-dithiolato)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 25787-92-2
(1,2-bis(diphenylphosphane)ethane)carbonateplatinum(II)

: 584-04-3
1,3-dimercapto-2-propanol

: 1280725-13-4
cis-(1,2-bis(diphenylphosphino)ethane)(2-hydroxypropane-1,3-dithiolato)platinum(II)

Guidance literature:: In acetone; (Ar) dithiol was added to soln. Pt complex in acetone, stirred at room temp. for 15 h; solvent was removed in vacuo, chromy. on silica (CHCl3-THF) and recrystn. from CH2Cl2-pentane; elem. anal.;
DOI:10.1039/c0dt00845a

Reference yield: 46.0%

: 10199-34-5,14056-88-3,15604-36-1
cis-dichlorobis(triphenylphosphine)platinum(II)

: 64-17-5
ethanol

: 584-04-3
1,3-dimercapto-2-propanol

: 1280725-13-4
cis-(1,2-bis(diphenylphosphino)ethane)(2-hydroxypropane-1,3-dithiolato)platinum(II)

: 1280725-14-5
cis-(1,2-bis(diphenylphosphino)ethane)(3-ethoxypropane-1,2-dithiolato)platinum(II)

Guidance literature:: With potassium carbonate; In ethanol; (Ar) dithiol was added to suspn. Pt complex and K2CO3 in EtOH, stirred at room temp. for 15 h and heated to 78°C for 6 h; solvent was removed in vacuo, residue was extd. with CHCl3-H2O, org. layer was dried over Na2SO4, filtered and evapd. in vacuo, chromy. on silica (CHCl3-THF) and recrystn. from CH2Cl2-pentane; elem. anal.;
DOI:10.1039/c0dt00845a