2C₅H₅N*Br₂Zn

Base Information

Chemical Name:2C₅H₅N*Br₂Zn
CAS No.:82009-22-1
Molecular Formula:Br₂Zn*2C₅H₅N
Molecular Weight:383.401
Hs Code.:

2C<sub>5</sub>H<sub>5</sub>N*Br<sub>2</sub>Zn

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2C₅H₅N*Br₂Zn

Chemical Property:

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Technology Process of 2C₅H₅N*Br₂Zn

There total 13 articles about 2C₅H₅N*Br₂Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1272-71-5
bis(mesitylene)vanadium⁽⁰⁾

: 25377-37-1,27790-75-6,82009-22-1
Tetrakis(pyridin)-dichlorovanadin(II)

: 108-67-8
1,3,5-trimethyl-benzene

Guidance literature:: With pyridine; 3-chloroprop-1-ene; In toluene; soln. of V-complex in toluene was treated with CH2=CHCH2Cl (inert atmosphere), the mixt. was stirred at room temp. for 24 h; the mother liquor contained org. compounds, products of the reaction of CH2=CHCH2Cl with either toluene or mesitylene (CLG-MS); filtered, ppt. was dissolved in pyridine, soln. was filtered and concd.to give the crystals of VCl2*4Py; identified by comparison of the IR spectrum with that of authentic sample;
DOI:10.1016/0022-328X(83)80106-5

Reference yield: 47.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 111-25-1
1-bromo-hexane

: 28665-60-3
(E)-1-phenyl-1-octene

: 25377-37-1,27790-75-6,82009-22-1
2C₅H₅N*Br₂Zn

Guidance literature:: With pyridine; zinc; bis(triphenylphosphine)nickel(II) chloride; In acetonitrile; at 65 ℃; for 4h;

Reference yield: 45.0%

: 131063-11-1,16997-51-6,19559-06-9
Vanadium (III) chloride-(tris-tetrahydrofuran)

: 13170-43-9
(trimethylsilyl)methylmagnesium chloride

: 25377-37-1,27790-75-6,82009-22-1
Tetrakis(pyridin)-dichlorovanadin(II)

: 41572-08-1
tetrakis(trimethylsilylmethyl)vanadium

: 7786-30-3
magnesium chloride

Guidance literature:: In diethyl ether; 1 mol of complex was slowly added to an ether soln. of 2 mol RMgCl at -15°C, after 1 h the temp. was raised to room temp. (Ar atm.);; dioxane was added, ppt. was extd. with pentane; elem. anal.;;
DOI:10.1016/S0022-328X(00)82672-8