trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammoniumiodide

Base Information

Chemical Name:trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammoniumiodide
CAS No.:854497-24-8
Molecular Formula:C₂₆H₂₉FeNOP*I
Molecular Weight:585.248
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammoniumiodide

Chemical Property:

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Technology Process of trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammoniumiodide

There total 2 articles about trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammoniumiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 854497-20-4,541540-61-8
[2-(N,N-dimethylaminomethyl)ferrocenyl]diphenylphosphine oxide

: 74-88-4
methyl iodide

: 854497-24-8
trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammoniumiodide

Guidance literature:: In methanol; (inert atm.); addn. of excess CH3I to a soln. of iron complex in methanol at room temp., heating at 60°C for 10 min, cooling to room temp.; addn. of ether with stirring, standing for crystn.; not purified;

Reference yield:

: 541540-61-8,854497-20-4
(R)-[2-(N,N-dimethylaminomethyl)ferrocenyl]diphenylphosphine oxide

: 74-88-4
methyl iodide

: 854497-24-8
(R)-trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammonium iodide

Guidance literature:: In not given;

Reference yield: 57.0%

: 854497-24-8
trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammoniumiodide

: 121-45-9
phosphorous acid trimethyl ester

: 854497-28-2,854497-36-2
dimethyl [2-(diphenylphosphinyl)ferrocenyl]methyl phosphonate

Guidance literature:: In xylene; (inert atm.); heating a soln. of iron complex and phosphite in xylene at145°C for 2.5 h; evapn., dissolving in CH2Cl2, chromy. (alumina, ether/methanol 95:5); elem. anal.;