dimethyl [2-(diphenylphosphinyl)ferrocenyl]methyl phosphonate

Base Information

Chemical Name:dimethyl [2-(diphenylphosphinyl)ferrocenyl]methyl phosphonate
CAS No.:854497-28-2
Molecular Formula:C₂₅H₂₆FeO₄P₂
Molecular Weight:508.274
Hs Code.:

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Chemical Property of dimethyl [2-(diphenylphosphinyl)ferrocenyl]methyl phosphonate

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Technology Process of dimethyl [2-(diphenylphosphinyl)ferrocenyl]methyl phosphonate

There total 1 articles about dimethyl [2-(diphenylphosphinyl)ferrocenyl]methyl phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 854497-24-8
trimethyl[(2-diphenylphosphinyl)ferrocenylmethyl]ammoniumiodide

: 121-45-9
phosphorous acid trimethyl ester

: 854497-28-2,854497-36-2
dimethyl [2-(diphenylphosphinyl)ferrocenyl]methyl phosphonate

Guidance literature:: In xylene; (inert atm.); heating a soln. of iron complex and phosphite in xylene at145°C for 2.5 h; evapn., dissolving in CH2Cl2, chromy. (alumina, ether/methanol 95:5); elem. anal.;

Reference yield: 70.0%

: 854497-28-2,854497-36-2
dimethyl [2-(diphenylphosphinyl)ferrocenyl]methyl phosphonate

: 10025-78-2
trichlorosilane

: 854497-22-6
[2-(phosphinomethyl)ferrocenyl]diphenylphosphine

Guidance literature:: With triethylamine; In toluene; (inert atm.); addn. of a soln. of iron complex in toluene to a soln. of silicon compd. in toluene at 0°C, addn. of excess of amine, heating in a sealed glass tube at 120°C for 5 h, cooling to room temp.; addn. of aq. NaOH, extn. with CH2Cl2, washing org. layer with water, drying (MgSO4), column chromy. (alumina, cyclohexane/ether 94:6); elem. anal.;