1-benzyl-3-methoxy-5-oxo-3,4-dehydropiperidine oxime

Base Information

Chemical Name:1-benzyl-3-methoxy-5-oxo-3,4-dehydropiperidine oxime
CAS No.:78156-37-3
Molecular Formula:C₁₃H₁₆N₂O₂
Molecular Weight:232.282
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-3-methoxy-5-oxo-3,4-dehydropiperidine oxime

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Technology Process of 1-benzyl-3-methoxy-5-oxo-3,4-dehydropiperidine oxime

There total 1 articles about 1-benzyl-3-methoxy-5-oxo-3,4-dehydropiperidine oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-56-1
methanol

: 50866-56-3
1-(benzyl)piperidin-3,5-dione

: 78156-37-3
1-benzyl-3-methoxy-5-oxo-3,4-dehydropiperidine oxime

Guidance literature:: With hydroxylamine hydrochloride;

Reference yield:

: 78156-37-3
1-benzyl-3-methoxy-5-oxo-3,4-dehydropiperidine oxime

: 64436-92-6
3-amino-5-methoxypyridine

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine

2: 75 percent

3: 73 percent / H₂ / 5percent Pd/C / 3040 Torr / Ambient temperature

4: 67 percent / aq. NaOH / 1 h / 65 °C

With pyridine; sodium hydroxide; hydrogen; palladium on activated charcoal;