[((CH₃)3Si)2NC(N(C₆H₁₁))2]BCl₂

Base Information

Chemical Name:[((CH₃)3Si)2NC(N(C₆H₁₁))2]BCl₂
CAS No.:883561-95-3
Molecular Formula:C₁₉H₄₀BCl₂N₃Si₂
Molecular Weight:448.435
Hs Code.:

[((CH<sub>3</sub>)3Si)2NC(N(C<sub>6</sub>H<sub>11</sub>))2]BCl<sub>2</sub>

Synonyms:

Suppliers and Price of [((CH₃)3Si)2NC(N(C₆H₁₁))2]BCl₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [((CH₃)3Si)2NC(N(C₆H₁₁))2]BCl₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [((CH₃)3Si)2NC(N(C₆H₁₁))2]BCl₂

There total 2 articles about [((CH₃)3Si)2NC(N(C₆H₁₁))2]BCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 6591-26-0
bis(trimethylsilyl)aminodichloroborane

: 538-75-0
dicyclohexyl-carbodiimide

: 883561-95-3
[((CH₃)3Si)2NC(N(C₆H₁₁))2]BCl₂

Guidance literature:: In diethyl ether; hexane; all manipulations under dry, oxygen-free Ar atm.; soln. of B compd. in hexane added to soln. of org. compd. in Et2O at ambient temp., stirred overnight at room temp.; solvent removed in vac.; elem. anal.;
DOI:10.1016/j.poly.2005.11.012

Reference yield: 77.0%

: 10294-34-5
boron trichloride

: 538-75-0
dicyclohexyl-carbodiimide

: 4039-32-1
lithium hexamethyldisilazane

: 883561-95-3
[((CH₃)3Si)2NC(N(C₆H₁₁))2]BCl₂

Guidance literature:: In diethyl ether; hexane; all manipulations under dry, oxygen-free Ar atm.; soln. of Li compd. in Et2O added to cold (-78°C) soln. of org. compd. in hexane, stirred mixt. warmed to room temp., cooled to -78°C, B compd. added dropwise, stirred for 2 h at room temp.; filtered, solvent stripped from filtrate, recrystd. from toluene at -40°C; elem. anal.;
DOI:10.1016/j.poly.2005.11.012