bis(trimethylsilyl)diethylgermane

Base Information

Chemical Name:bis(trimethylsilyl)diethylgermane
CAS No.:104585-86-6
Molecular Formula:C₁₀H₂₈GeSi₂
Molecular Weight:277.093
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(trimethylsilyl)diethylgermane

Chemical Property:

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Technology Process of bis(trimethylsilyl)diethylgermane

There total 2 articles about bis(trimethylsilyl)diethylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.6%

: 75-77-4
chloro-trimethyl-silane

: 6727-87-3
triethylgermyllithium

: 104585-84-4
trimethylsilyldiethylgermyllithium

: 104585-86-6
bis(trimethylsilyl)diethylgermane

: 993-84-0
pentaethyldigermane

: 1631-46-5
diethylgermane

: 1188-14-3
Triethylgerman

: 7749-85-1
trimethylsilyltriethylgermane

Guidance literature:: With water; In N,N,N,N,N,N-hexamethylphosphoric triamide; Equimolar mixt. of Et3GeLi and Me3SiGeEt2Li in HMPA is stirred for 94 h at 25°C, then Me3SiCl and water are added.; extn. with ether;
DOI:10.1016/0022-328X(81)80004-6

Reference yield:

: 6727-87-3
triethylgermyllithium

: 104585-84-4
trimethylsilyldiethylgermyllithium

: 100460-02-4
trimethylsilyldiethylgermane

: 104585-86-6
bis(trimethylsilyl)diethylgermane

: 993-84-0
pentaethyldigermane

: 1188-14-3
Triethylgerman

: 7749-85-1
trimethylsilyltriethylgermane

Guidance literature:: With water; In N,N,N,N,N,N-hexamethylphosphoric triamide; byproducts: (C2H5)2GeH2; react. in evacuated quartz tube, equimolar mixt. of Et3GeLi and Me3SiGeEt2Li stirred for 94 h at 25°C; hydrolysis; extn. with ether; not isolated, detected by GLC and mass spectrometry;