4-[(Methylamino)acetyl]morpholine

Base Information

• Chemical Name: 4-[(Methylamino)acetyl]morpholine
• CAS No.: 41458-73-5
• Molecular Formula: C7H14N2O2
• Molecular Weight: 158.2
• European Community (EC) Number: 255-381-8
• Nikkaji Number: J320.079E
• Mol file: 41458-73-5.mol

Synonyms:41458-73-5;4-[(Methylamino)acetyl]morpholine;2-(Methylamino)-1-morpholinoethanone;EINECS 255-381-8;2-(methylamino)-1-(morpholin-4-yl)ethan-1-one;2-(methylamino)-1-morpholin-4-ylethanone;4-((Methylamino)acetyl)morpholine;C7H14N2O2;Morpholine, 4-((methylamino)acetyl)-;sarcosine morpholide;SCHEMBL1484933;BHUKCEYZKFAGEY-UHFFFAOYSA-N;HMS1732J07;STL138422;AKOS000210223;2-methylamino-1-morpholin-4-ylethanone;2-methylamino-1-morpholin-4-ylmethanone;2-(Methylamino)-1-morpholinoethan-1-one;2-(methylamino)-1-(morpholin-4-yl)ethanone;CS-0301435;EN300-34301;AS-787/43399851;N-methyl-N-[2-(4-morpholinyl)-2-oxoethyl]amine;Z56347542

Chemical Property of 4-[(Methylamino)acetyl]morpholine

Chemical Property:

• Vapor Pressure: 0.00167mmHg at 25°C
• Refractive Index: 1.477
• Boiling Point: 294 °C at 760 mmHg
• Flash Point: 131.6 °C
• Density: 1.09 g/cm³
• XLogP3: -1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 158.105527694
• Heavy Atom Count: 11
• Complexity: 132

Purity/Quality:

97% ^*data from raw suppliers

2-Methylamino-1-morpholin-4-yl-ethanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNCC(=O)N1CCOCC1

Technology Process of 4-[(Methylamino)acetyl]morpholine

There total 1 articles about 4-[(Methylamino)acetyl]morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-chloroacetylmorpholine (1440-61-5) + methylamine (74-89-5) → N-Methylglycylmorpholid (41458-73-5)

Guidance literature:

With benzene;

Reference yield: 63.0%

13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid (877291-09-3) + N-Methylglycylmorpholid (41458-73-5) → 6-[[(carboxymethyl)methylamino]carbonyl]-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid + 13-cyclohexyl-3-methoxy-6-[[methyl[2-(4-morpholinyl)-2-oxoethyl]amino]carbonyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid

Guidance literature:

13-cyclohexyl-3-(methyloxy)-10-((methyloxy)carbonyl)-7H-indolo[2,1-a][2]benzazepine-6-carboxylic acid; N-Methylglycylmorpholid; With triethylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

With methanol; sodium hydroxide; water; In tetrahydrofuran; at 85 ℃; for 0.333333h; Microwave irradiation;

With hydrogenchloride; In tetrahydrofuran; methanol; water;

Reference yield:

N-Methylglycylmorpholid (41458-73-5) + 4-nitro-benzoyl chloride (122-04-3) → C14H17N3O5 (1251942-62-7)

Guidance literature:

With potassium carbonate; In acetonitrile; at 60 - 85 ℃; for 12h;

DOI:10.1016/j.bmcl.2010.03.074

upstream raw materials:

N-chloroacetylmorpholine

methylamine

Downstream raw materials:

C₁₄H₁₇N₃O₅

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