bis(triphenylphosphine)nitrogen diphenoxo(phthalocyaninato)ferrate(III)

Base Information

Chemical Name:bis(triphenylphosphine)nitrogen diphenoxo(phthalocyaninato)ferrate(III)
CAS No.:102588-66-9
Molecular Formula:C₃₆H₃₀NP₂*C₄₄H₂₆FeN₈O₂
Molecular Weight:1293.18
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(triphenylphosphine)nitrogen diphenoxo(phthalocyaninato)ferrate(III)

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Technology Process of bis(triphenylphosphine)nitrogen diphenoxo(phthalocyaninato)ferrate(III)

There total 2 articles about bis(triphenylphosphine)nitrogen diphenoxo(phthalocyaninato)ferrate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {N(P(C₆H₅)3)2}⁽¹⁺⁾*{Fe(OH)2(C₃₂H₁₆N₈)}^(1-)={N(P(C₆H₅)3)2}{Fe(OH)2(C₃₂H₁₆N₈)}

: 108-95-2,27073-41-2
phenol

: 102588-66-9
bis(triphenylphosphine)nitrogen diphenoxo(phthalocyaninato)ferrate(III)

Guidance literature:: In dichloromethane; soln. of Fe-complex is mixed with soln. of phenol, addn. of ether causes precipitation of black crystals; recrystn. from CH2Cl2/ether;

Reference yield:

: 14285-56-4
iron(III)phthalocyanine chloride

: 100-67-4
potassium phenolate

: 65300-04-1
bis(triphenylphosphane)iminium perchlorate

: 102588-66-9
bis(triphenylphosphine)nitrogen diphenoxo(phthalocyaninato)ferrate(III)

Guidance literature:: In dichloromethane; byproducts: KClO4; potassium phenolate (from potassium and dry phenol in toluene) is suspended in CH2Cl2, addn. of (PNP)ClO4, filtn., mixing with Fe-complex, stirring till the Fe-complex is dissolved; filtn., mixing with ether for crystallization of product, recrystn. at -25°C, elem. anal.;