benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate

Base Information

Chemical Name:benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate
CAS No.:145100-54-5
Molecular Formula:C16H19NO3
Molecular Weight:273.332
Hs Code.:2933399090
DSSTox Substance ID:DTXSID10439004
Nikkaji Number:J574.246C
Mol file:145100-54-5.mol

Synonyms:145100-54-5;benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate;Benzyl 4-oxo-2-propyl-2,3-dihydropyridine-1-carboxylate;Benzyl 2-n-propyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate;DTXSID10439004;SYWFGYZHYRYOKS-UHFFFAOYSA-N;Benzyl4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate;1(2H)-Pyridinecarboxylic acid, 3,4-dihydro-4-oxo-2-propyl-, phenylmethyl ester;FT-0740400;A850633;J-503020;1-(Benzyloxycarbonyl)-2-propyl-1,2,3,4-tetrahydropyridine-4-one;BENZYL2-N-PROPYL-4-OXO-3,4-DIHYDROPYRIDINE-1(2H)-CARBOXYLATE

Suppliers and Price of benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
Benzyl2-n-propyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95
10g
$ 2933.00

Crysdot
Benzyl4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate 95+%
1g
$ 614.00

Chemenu
benzyl4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate 95%
1g
$ 580.00

American Custom Chemicals Corporation
BENZYL 4-OXO-2-PROPYL-3,4-DIHYDROPYRIDINE-1(2H)-CARBOXYLATE 95.00%
5MG
$ 503.99

Alichem
Benzyl4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate
1g
$ 535.00

Total 13 raw suppliers

Chemical Property of benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate

Chemical Property:

PSA：46.61000
LogP:3.21830
Storage Temp.:2-8°C
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:273.13649347
Heavy Atom Count:20
Complexity:372

Purity/Quality:

97% ^*data from raw suppliers

Benzyl2-n-propyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC1CC(=O)C=CN1C(=O)OCC2=CC=CC=C2

Technology Process of benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate

There total 7 articles about benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 927-77-5
n-propylmagnesium bromide

: 1-Benzyloxycarbonyl-4-methoxy-pyridinium; chloride

: 145100-54-5
benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate

Guidance literature:: With oxonium;
DOI:10.1016/S0040-4039(98)01195-2

Reference yield:

: 620-08-6,1232006-56-2
4-methoxypyridine

: 2234-82-4
1-propylmagnesium chloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 145100-54-5
benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate

Guidance literature:: With copper(l) chloride; In tetrahydrofuran; diethyl ether; at 0 ℃; Inert atmosphere;
DOI:10.1002/anie.200904981

Reference yield:

: benzyl 4-oxopyridine-1(4H)-carboxylate

: 927-77-5
n-propylmagnesium bromide

: 145100-54-5
benzyl 4-oxo-2-propyl-3,4-dihydropyridine-1(2H)-carboxylate

Guidance literature:: benzyl 4-oxopyridine-1(4H)-carboxylate; With copper(I) bromide dimethylsulfide complex; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In dichloromethane; at 18 - 25 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere; Schlenk technique;

n-propylmagnesium bromide; In dichloromethane; at -78 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201906237