(But-3-yn-1-yl)dimethylamine

Base Information

• Chemical Name: (But-3-yn-1-yl)dimethylamine
• CAS No.: 14731-37-4
• Molecular Formula: C6H11N
• Molecular Weight: 97.16
• European Community (EC) Number: 820-888-0
• DSSTox Substance ID: DTXSID00903800
• Nikkaji Number: J1.979.756B
• Mol file: 14731-37-4.mol

Synonyms:(but-3-yn-1-yl)dimethylamine;14731-37-4;N,N-dimethylbut-3-yn-1-amine;N,N-Dimethyl-3-butyn-1-amine;NoName_4551;but-3-ynyl-dimethyl-amine;DTXSID00903800;WSCWSMUKWIYUFV-UHFFFAOYSA-N;AC9551;MFCD18851244;AKOS012966933;SY261953;EN300-91739

Chemical Property of (But-3-yn-1-yl)dimethylamine

Chemical Property:

• Vapor Pressure: 29.619mmHg at 25°C
• XLogP3: 0.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 97.089149355
• Heavy Atom Count: 7
• Complexity: 75.4

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)CCC#C

Technology Process of (But-3-yn-1-yl)dimethylamine

There total 1 articles about (But-3-yn-1-yl)dimethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-butyn-1-yl p-toluenesulfonate (23418-85-1) + dimethyl amine (124-40-3) → N,N-dimethylbut-3-yn-1-amine (14731-37-4)

Guidance literature:

In water; at 20 ℃; for 16h;

DOI:10.1021/ol0341039

Reference yield: 34.0%

N-(4-chlorobenzyl)-4-hydroxy-8-iodo-6-(4-morpholinylmethyl)-3-quinolinecarboxamide + N,N-dimethylbut-3-yn-1-amine (14731-37-4) → N-(4-chlorobenzyl)-2-[2-(dimethylamino)ethyl]-8-(morpholin-4-ylmethyl)-6-oxo-6H-pyrrolo[3,2,1-ij]quinoline-5-carboxamide (1027379-57-2)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In ethanol; N,N-dimethyl-formamide; Reflux;

DOI:10.1016/j.bmcl.2010.03.115

Reference yield:

4-fluoro-3-nitrophenylazide (28166-06-5) + N,N-dimethylbut-3-yn-1-amine (14731-37-4) → 2-(1-(4-fluoro-3-nitrophenyl)-1H-1,2,3-triazol-4-yl)-N,N-dimethylethanamine

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 16h;

upstream raw materials:

3-butyn-1-yl p-toluenesulfonate

dimethyl amine

Downstream raw materials:

trimethyl-oct-3-ynyl-ammonium; iodide

5-Hydroxy-5,5-diphenyl-pentin-(3)-yl-

9-Hydroxy-9-<4-dimethylamino-butin-(1)-yl>-fluoren

5-Dimethylamino-1-cyclohexyl-1-phenyl-pentin-(2)-ol-(1)