propan-2-yl piperidine-1-carboxylate

Base Information

• Chemical Name: propan-2-yl piperidine-1-carboxylate
• CAS No.: 6301-08-2
• Molecular Formula: C₉H₁₇NO₂
• Molecular Weight: 171.239

Synonyms:1-Piperidinecarboxylicacid, isopropyl ester (7CI,8CI); 1-(Isopropoxycarbonyl)piperidine;N-(1-Methylethoxycarbonyl)piperidine; NSC 44153

Chemical Property of propan-2-yl piperidine-1-carboxylate

Chemical Property:

• Vapor Pressure: 0.0637mmHg at 25°C
• Boiling Point: 231°C at 760 mmHg
• Flash Point: 93.5°C
• Density: 1.016g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of propan-2-yl piperidine-1-carboxylate

There total 4 articles about propan-2-yl piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

piperidine (110-89-4) + carbon monoxide (201230-82-2) + isopropyl alcohol (67-63-0,8013-70-5) → isopropyl piperidine-1-carboxylate (6301-08-2)

Guidance literature:

With 2C₇H₉N₄*Au⁽¹⁺⁾*Cu⁽¹⁺⁾*2I^(1-); In toluene; at 90 ℃; for 24h; Time; Autoclave;

DOI:10.1002/anie.201914089

Reference yield: 69.8%

piperidine (110-89-4) + chloromethyl isopropyl carbonate (35180-01-9) → isopropyl piperidine-1-carboxylate (6301-08-2)

Guidance literature:

In benzene; a.) RT, 1 h, b.) reflux, 1 h;

Reference yield:

piperidine (110-89-4) + isopropyl chloroformate (108-23-6) → isopropyl piperidine-1-carboxylate (6301-08-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene; at 20 ℃;

DOI:10.1016/j.tetlet.2021.152978

upstream raw materials:

piperidine

chloromethyl isopropyl carbonate

carbon dioxide

isopropyl bromide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 6301-08-2 propan-2-yl piperidine-1-carboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send