7-hydroxy-7-cyanomethyl-benzo-2-furanone

Base Information

• Chemical Name: 7-hydroxy-7-cyanomethyl-benzo-2-furanone
• CAS No.: 190851-63-9
• Molecular Formula: C₁₀H₇NO₃
• Molecular Weight: 189.17

Synonyms:

Chemical Property of 7-hydroxy-7-cyanomethyl-benzo-2-furanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-hydroxy-7-cyanomethyl-benzo-2-furanone

There total 3 articles about 7-hydroxy-7-cyanomethyl-benzo-2-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 3-phenyliodonio-1,4-naphthoquinone-2-imide (175348-70-6) → 2-amino-3-iodonaphthalene-1,4-dione (175348-78-4) + 7-hydroxy-7-cyanomethyl-benzo-2-furanone (190851-63-9) + 3-iodo-2-phenylamino-1,4-naphthoquinone + 2-(2-Cyano-acetyl)-benzoic acid methyl ester

Guidance literature:

With sodium; for 24h;

DOI:10.1016/S0040-4020(97)00270-6

Reference yield:

propan-1-ol (71-23-8) + 3-phenyliodonio-1,4-naphthoquinone-2-imide (175348-70-6) → 2-amino-3-iodonaphthalene-1,4-dione (175348-78-4) + 7-hydroxy-7-cyanomethyl-benzo-2-furanone (190851-63-9) + 3-iodo-2-phenylamino-1,4-naphthoquinone + 2-(2-Cyano-acetyl)-benzoic acid propyl ester

Guidance literature:

With sodium; for 24h;

DOI:10.1016/S0040-4020(97)00270-6

Reference yield:

ethanol (64-17-5) + 3-phenyliodonio-1,4-naphthoquinone-2-imide (175348-70-6) → 2-amino-3-iodonaphthalene-1,4-dione (175348-78-4) + 7-hydroxy-7-cyanomethyl-benzo-2-furanone (190851-63-9) + 3-iodo-2-phenylamino-1,4-naphthoquinone + 2-(2-Cyano-acetyl)-benzoic acid ethyl ester

Guidance literature:

With sodium; for 24h;

DOI:10.1016/S0040-4020(97)00270-6

upstream raw materials:

methanol

3-phenyliodonio-1,4-naphthoquinone-2-imide

propan-1-ol

ethanol

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