Trisulfide, dicyclohexyl

Base Information

• Chemical Name: Trisulfide, dicyclohexyl
• CAS No.: 15619-03-1
• Molecular Formula: C12H22S3
• Molecular Weight: 262.505
• Mol file: 15619-03-1.mol

Synonyms:

Chemical Property of Trisulfide, dicyclohexyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Trisulfide, dicyclohexyl

There total 10 articles about Trisulfide, dicyclohexyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

cyclohexyl tosylate (953-91-3) → C12H22S3 (15619-03-1)

Guidance literature:

With potassium 5-methyl-1,3,4-oxadiazole-2-thiolate; In water; at 40 ℃; for 2h;

DOI:10.1080/17415993.2016.1253696

Reference yield: 74.0%

Cyclohexanethiol (1569-69-3) → C12H22S3 (15619-03-1)

Guidance literature:

Cyclohexanethiol; With triethylamine; In propan-1-ol; at 20 ℃; for 0.333333h;

With 3,4-dichloro-1,2,5-thiadiazole; In propan-1-ol; for 0.833333h;

DOI:10.1080/17415993.2021.1991928

Reference yield:

cyclohexane (110-82-7,25012-93-5) → 1,2-dicyclohexyl disulfide (2550-40-5) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + C12H22S3 (15619-03-1) + cyclohexanol (108-93-0)

Guidance literature:

With hydrogen sulfide; oxygen; iron; In pyridine; acetic acid; Product distribution; Mechanism; Kinetics; Ambient temperature; iron catalyzed insertion of sulfur into the non-activated C-H bond; variation of the sulfur reagent, the catalyst and of the AcOH conc.; or in CF₃COOH; or with other cyclic hydrocarbons;

DOI:10.1016/S0040-4020(01)88512-4

upstream raw materials:

cyclohexane

cyclohexyl tosylate

Cyclohexanethiol

1,2-dicyclohexyl disulfide

Downstream raw materials:

dicyclohexyl tetrasulfide