4-(Prop-2-en-1-yl)benzene-1,3-diol

Base Information

• Chemical Name: 4-(Prop-2-en-1-yl)benzene-1,3-diol
• CAS No.: 1616-52-0
• Molecular Formula: C9H10O2
• Molecular Weight: 150.177
• DSSTox Substance ID: DTXSID60552015
• Nikkaji Number: J765.261E
• Wikidata: Q82431973
• Mol file: 1616-52-0.mol

Synonyms:1616-52-0;4-(Prop-2-en-1-yl)benzene-1,3-diol;1,3-Benzenediol, 4-(2-propen-1-yl)-;4-allylbenzene-1,3-diol;4-allylresorcinol;4-prop-2-enylbenzene-1,3-diol;SCHEMBL69697;DTXSID60552015;AKOS015995592

Chemical Property of 4-(Prop-2-en-1-yl)benzene-1,3-diol

Chemical Property:

• XLogP3: 1.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 150.068079557
• Heavy Atom Count: 11
• Complexity: 134

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCC1=C(C=C(C=C1)O)O

Technology Process of 4-(Prop-2-en-1-yl)benzene-1,3-diol

There total 11 articles about 4-(Prop-2-en-1-yl)benzene-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

allyl alcohol (107-18-6) + recorcinol (108-46-3) → 2,4-diallyl-1,3-benzenediol (71489-64-0) + 4-allyl-1,3-dihydroxybenzene (1616-52-0) + 2-allyl-1,3-dihydroxybenzene (1746-89-0)

Guidance literature:

With triethyl borane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; toluene; at 20 ℃;

DOI:10.1055/s-2006-950220

Reference yield: 77.0%

allyl alcohol (107-18-6) + recorcinol (108-46-3) → 4-allyl-1,3-dihydroxybenzene (1616-52-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethyl borane; In tetrahydrofuran; hexane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1039/b927558d

Reference yield: 62.0%

3-chloroprop-1-ene (107-05-1) + recorcinol (108-46-3) → 4-allyl-1,3-dihydroxybenzene (1616-52-0)

Guidance literature:

With sodium carbonate; copper(l) chloride; In water; at 20 ℃; for 0.5h;

DOI:10.1248/CPB.C20-00294

upstream raw materials:

3-allyloxyphenol

resorcinol; sodium-compound

3-chloroprop-1-ene

N,N-diethylaniline

Downstream raw materials:

4-propylresorcinol

Osmorhizole

1-Allyl-2,4-bis-benzyloxy-benzene

5-allyl-2,4-dihydroxybenzaldehyde