(2-Hydroxy-5-methoxyphenyl)(4-methoxyphenyl)methanone

Base Information

• Chemical Name: (2-Hydroxy-5-methoxyphenyl)(4-methoxyphenyl)methanone
• CAS No.: 16762-04-2
• Molecular Formula: C15H14O4
• Molecular Weight: 258.274
• DSSTox Substance ID: DTXSID80401213
• Wikidata: Q82204273
• Mol file: 16762-04-2.mol

Synonyms:ST51009822;16762-04-2;SCHEMBL6374455;DTXSID80401213;UWLCYNYSVSFDPX-UHFFFAOYSA-N;AKOS024372254;(2-Hydroxy-5-methoxyphenyl)(4-methoxyphenyl)methanone

Chemical Property of (2-Hydroxy-5-methoxyphenyl)(4-methoxyphenyl)methanone

Chemical Property:

• Melting Point: 71°C
• PSA: 55.76000
• LogP: 2.64040
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 258.08920892
• Heavy Atom Count: 19
• Complexity: 297

Purity/Quality:

(2-HYDROXY-5-METHOXYPHENYL)-(4-METHOXYPHENYL)METHANONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C(=O)C2=C(C=CC(=C2)OC)O

Technology Process of (2-Hydroxy-5-methoxyphenyl)(4-methoxyphenyl)methanone

There total 7 articles about (2-Hydroxy-5-methoxyphenyl)(4-methoxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(2,5-dimethoxyphenyl)(4-methoxyphenyl)methanone (80427-23-2) → 2-hydroxy-4',5-dimethoxybenzophenone (16762-04-2)

Guidance literature:

With beryllium(II) chloride; In toluene; for 3h; Heating;

DOI:10.1016/0040-4020(96)00815-0

Reference yield: 60.0%

(2,5-dihydroxyphenyl)(4-hydroxyphenyl)methanone (120506-56-1) + methyl iodide (74-88-4) → 2-hydroxy-4',5-dimethoxybenzophenone (16762-04-2)

Guidance literature:

With potassium carbonate; In acetone; for 6h; Heating / reflux;

Reference yield: 52.0%

4-methoxyphenyl 4-methoxybenzoate (60127-34-6) → 2-hydroxy-4',5-dimethoxybenzophenone (16762-04-2)

Guidance literature:

With aluminum (III) chloride; In N,N-dimethyl-formamide; at 210 ℃; for 3h;

DOI:10.5012/bkcs.2012.33.6.1939

upstream raw materials:

4-methoxyphenyl 4-methoxybenzoate

(2,5-dimethoxyphenyl)(4-methoxyphenyl)methanone

4-methoxy-benzoyl chloride

1,4-dimethoxybezene

Downstream raw materials:

2-(4-methoxybenzoyloxy)-4',5-dimethoxybenzophenone

(3-bromo-2-hydroxy-5-methoxyphenyl)(4-methoxyphenyl)-methanone

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