Silane, (4-chlorophenoxy)trimethyl-

Base Information

• Chemical Name: Silane, (4-chlorophenoxy)trimethyl-
• CAS No.: 17005-59-3
• Molecular Formula: C9H13ClOSi
• Molecular Weight: 200.74
• Mol file: 17005-59-3.mol

Synonyms:Silane, (4-chlorophenoxy)trimethyl-;(4-chlorophenoxy)triisopropylsilane;p-chlorophenoxy trimethylsilane;(4-chlorophenoxy)trimethylsilane;4-Cl-C6H4OTMS;trimethyl(4-chlorophenoxy)silane;trimethyl-p-chlorophenoxysilane;

Chemical Property of Silane, (4-chlorophenoxy)trimethyl-

Chemical Property:

• Refractive Index: 1.4930
• Boiling Point: 214°C
• PSA: 9.23000
• Density: 1.0320
• LogP: 3.55370

Purity/Quality:

(4-Chlorophenoxy)triisopropylsilane 98 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Silane, (4-chlorophenoxy)trimethyl-

There total 11 articles about Silane, (4-chlorophenoxy)trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-chloro-phenol (106-48-9,82344-39-6) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → 4-chlorophenoxytrimethylsilane (17005-59-3)

Guidance literature:

With aluminum potassium sulfate dodecahydrate; In acetonitrile; at 20 ℃; for 0.333333h;

Reference yield: 96.0%

triisopropylsilyl chloride (13154-24-0) + 4-chloro-phenol (106-48-9,82344-39-6) → 4-chlorophenoxytrimethylsilane (17005-59-3)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 25 ℃;

DOI:10.1016/j.tet.2004.10.103

Reference yield: 95.0%

4-chloro-phenol (106-48-9,82344-39-6) + lithium hexamethyldisilazane (4039-32-1) → 4-chlorophenoxytrimethylsilane (17005-59-3)

Guidance literature:

With N-chlorosaccharin; In neat (no solvent); at 20 ℃; for 0.0833333h;

DOI:10.1002/jccs.201300624

upstream raw materials:

chloro-trimethyl-silane

4-chloro-phenol

1,1,1,3,3,3-hexamethyl-disilazane

potassium 4-chlorophenoxide

Downstream raw materials:

trimethyl-(4-trimethylsilanyloxy-phenyl)-silane

ethyl-[4-(ethyl-dimethyl-silanyloxy)-phenyl]-dimethyl-silane

dimethyl-bis-(4-trimethylsilanyloxy-phenyl)-silane

4-chlorophenyl trifluoromethanesulfonate