2-Naphthaleneacetic acid, a-oxo-, methyl ester

Base Information

• Chemical Name: 2-Naphthaleneacetic acid, a-oxo-, methyl ester
• CAS No.: 170166-53-7
• Molecular Formula: C13H10O3
• Molecular Weight: 214.221
• Mol file: 170166-53-7.mol

Synonyms:

Chemical Property of 2-Naphthaleneacetic acid, a-oxo-, methyl ester

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Naphthalen-2-yl-oxo-aceticacidmethylester 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Naphthaleneacetic acid, a-oxo-, methyl ester

There total 24 articles about 2-Naphthaleneacetic acid, a-oxo-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methanol (67-56-1) + 2-Bromo-2'-acetonaphthone (613-54-7) → methyl 2'-naphthoylformate (170166-53-7)

Guidance literature:

With selenium(IV) oxide; for 48h; Heating;

DOI:10.1080/10426500601142114

Reference yield: 87.0%

methyl bromide (74-83-9) + 2-naphthylglyoxal (22115-06-6) → methyl 2'-naphthoylformate (170166-53-7)

Guidance literature:

With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; In water; at 60 ℃; for 2h; Sealed tube;

DOI:10.1080/00397911.2019.1600193

Reference yield: 81.0%

2,2-Bis-benzotriazol-1-yl-2-methoxy-1-naphthalen-2-yl-ethanone (170166-57-1) → methyl 2'-naphthoylformate (170166-53-7)

Guidance literature:

With Amberlite H⁺ ion exchange resin IR-120 HPC; water; In methanol; Heating;

upstream raw materials:

2,2-Bis-benzotriazol-1-yl-2-methoxy-1-naphthalen-2-yl-ethanone

methanol

2-Bromo-2'-acetonaphthone

monomethyl oxalyl chloride

Downstream raw materials:

N-(4-methoxy-benzylidene)-N'-(3-(naphthalen-2-yl)-quinoxalin-2-yl)hydrazine

methyl 2-((4-methoxyphenyl)amino)-2-(naphthalen-2-yl)acetate

(+)-(R)-methyl 2-hydroxy-2-(naphthalen-2-yl)-3-oxo-5-phenylpentanoate

methyl 2-hydroxy-2-(naphthalen-2-yl)-3-(2-phenyloxazol-5-yl)propanoate

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