Phosphine, (trimethylsilyl)-

Base Information

Chemical Name:Phosphine, (trimethylsilyl)-
CAS No.:17446-52-5
Molecular Formula:C3H11PSi
Molecular Weight:106.18
Hs Code.:
DSSTox Substance ID:DTXSID40413392
Nikkaji Number:J960.251H

Synonyms:Phosphine, (trimethylsilyl)-;trimethylsilylphosphine;Trimethylsilanyl-phosphane;17446-52-5;SCHEMBL991242;DTXSID40413392

Suppliers and Price of Phosphine, (trimethylsilyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Phosphine, (trimethylsilyl)-

Chemical Property:

Boiling Point:77.5 °C
PSA：13.59000
LogP:1.69640
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:106.036763883
Heavy Atom Count:5
Complexity:28.4

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)P

Technology Process of Phosphine, (trimethylsilyl)-

There total 3 articles about Phosphine, (trimethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 96555-88-3
[(1,2-bis(dicyclohexylphosphino)ethane)dichloronickel(II)]

: 15573-39-4
bis(trimethylsilyl)phosphine

: 75-77-4
chloro-trimethyl-silane

: 57603-40-4,115223-08-0
Ni(1,2-bis(dicyclohexylphosphino)ethane)2

: ((C₆H₁₁)2PCH₂CH₂P(C₆H₁₁)2Ni)2P₂*2C₆H₅CH₃

: 17446-52-5
trimethylphosphinosilane

: 7803-51-2
phosphan

Guidance literature:: In tetrahydrofuran; under Ar, stirred for 3 h at 20°C; removal of the volatiles, recrystn. from toluene at -78°C, dried in vac. (20°C, 1 h); detn. of intermediates by NMR-spectroscopy;

Reference yield: 59.0%

: 37504-45-3
dichloro[1,2-bis(diethylphosphino)ethane]nickel(II)

: 15573-39-4
bis(trimethylsilyl)phosphine

: 75-77-4
chloro-trimethyl-silane

: 54910-60-0
bis{1,2-bis(diethylphosphino)ethane}nickel⁽⁰⁾

: 96555-93-0
(((C₂H₅)2PCH₂CH₂P(C₂H₅)2)Ni)2P₂

: 17446-52-5
trimethylphosphinosilane

: 7803-51-2
phosphan

Guidance literature:: In tetrahydrofuran; under Ar, stirred at 20°C for 2 h; removal of the volatiles (20°C, vac.), recrystn. from n-pentane at -20°C; elem. anal.;

Reference yield: 31.0%

: 14647-23-5
1,2-bis(diphenylphosphino)ethane nickel(II) chloride

: 15573-39-4
bis(trimethylsilyl)phosphine

: 15628-25-8
Ni⁽⁰⁾(1,2-bis(diphenylphosphino)ethane)2

: (((C₆H₅)2PCH₂CH₂P(C₆H₅)2)Ni)2P₂*3C₆H₅CH₃

: 17446-52-5
trimethylphosphinosilane

: 7803-51-2
phosphan

Guidance literature:: In tetrahydrofuran; under Ar, stirred for 2 h at 20°C; volume reduced, cooled to -78°C for 2 d, pptn. of (DPPE)2Ni, evapn. of mother liquor, recrystn. from toluene at -20°C, dried in vac. (20°C, 1 h); elem. anal.;