Technology Process of Benzeneacetaldehyde, 3-methoxy-a-phenyl-4-(phenylmethoxy)-
There total 5 articles about Benzeneacetaldehyde, 3-methoxy-a-phenyl-4-(phenylmethoxy)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
diethyl ether;
for 0.5h;
Ambient temperature;
DOI:10.1248/cpb.44.1188
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzene / 1.) RT, 50 min, 2.) 70 deg C, 7 h
2: conc. aq. HCl / benzene; methanol; tetrahydrofuran / 7 h / Heating
3: 90 percent / tert-BuOK / dimethylsulfoxide / 18 h / Ambient temperature
4: 93.2 percent / BF3*Et2O / diethyl ether / 0.5 h / Ambient temperature
With
hydrogenchloride; boron trifluoride diethyl etherate; potassium tert-butylate;
In
tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide; benzene;
DOI:10.1248/cpb.44.1188
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzene / 1.) RT, 50 min, 2.) 70 deg C, 7 h
2: conc. aq. HCl / benzene; methanol; tetrahydrofuran / 7 h / Heating
3: 90 percent / tert-BuOK / dimethylsulfoxide / 18 h / Ambient temperature
4: 93.2 percent / BF3*Et2O / diethyl ether / 0.5 h / Ambient temperature
With
hydrogenchloride; boron trifluoride diethyl etherate; potassium tert-butylate;
In
tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide; benzene;
DOI:10.1248/cpb.44.1188
