1-[(4-Ethenylphenyl)methyl]-1,4,7-triazonane

Base Information

Chemical Name:1-[(4-Ethenylphenyl)methyl]-1,4,7-triazonane
CAS No.:182306-47-4
Molecular Formula:C15H23N3
Molecular Weight:245.368
Hs Code.:
DSSTox Substance ID:DTXSID00596251
Nikkaji Number:J843.311I
Wikidata:Q82491463
Mol file:182306-47-4.mol

Synonyms:1-[(4-Ethenylphenyl)methyl]-1,4,7-triazonane;182306-47-4;SCHEMBL1809141;DTXSID00596251;{mono-N-(4-vinylbenzyl)-1,4,7-triazacyclononane}

Suppliers and Price of 1-[(4-Ethenylphenyl)methyl]-1,4,7-triazonane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[(4-Ethenylphenyl)methyl]-1,4,7-triazonane

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:245.189197746
Heavy Atom Count:18
Complexity:224

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CC1=CC=C(C=C1)CN2CCNCCNCC2

Technology Process of 1-[(4-Ethenylphenyl)methyl]-1,4,7-triazonane

There total 1 articles about 1-[(4-Ethenylphenyl)methyl]-1,4,7-triazonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 4730-54-5
1,4,7-triazacyclononane

: 182306-47-4
(N-(4-vinylbenzyl)-1,4,7-triazacyclononane)

Guidance literature:: With lithium hydroxide; In ethanol; water; for 3h; Heating;
DOI:10.1002/1099-0682(200109)2001:9<2217::AID-EJIC2217>3.0.CO;2-L

Reference yield: 70.0%

: 67-56-1
methanol

: 7732-18-5
water

: 49539-99-3,49540-00-3
mercuric triflate

: 182306-47-4
(N-(4-vinylbenzyl)-1,4,7-triazacyclononane)

: [(N-(4-vinylbenzyl)-1,4,7-triazacyclononane)2Hg](OTf)2*9H₂O*2CH₃OH

Guidance literature:: In methanol; to a MeOH soln. of organic ligand methanol soln. of Hg(OTf)2 added dropwise over 30 min. in the dark, stirred at room temp. for 48 h; insoluble species filtered off, solvent removed, in N2-filled glove box addn. of MeOH and small amt. of ether, reaction mixt. stayed at room temp. for 2 min., ppt. filtered off, process repeated three times,evapn., dried in vac. over P2O5; elem. anal.;
DOI:10.1002/1099-0682(200109)2001:9<2217::AID-EJIC2217>3.0.CO;2-L

Reference yield:

: 67-56-1
methanol

: 54010-75-2
zinc trifluoromethanesulfonate

: 182306-47-4
(N-(4-vinylbenzyl)-1,4,7-triazacyclononane)

: [Zn(N-(4-vinylbenzyl)-1,4,7-triazacyclononane)2](OTf)2

Guidance literature:: In methanol; molar ratio Zn:ligand=1:2, stirring at room temp. for 48 h; filtration, removal of volatiles (vac.); elem. anal.;
DOI:10.1002/anie.199706421