2-(Tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene

Base Information

Chemical Name:2-(Tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene
CAS No.:188345-71-3
Molecular Formula:C11H17NO2
Molecular Weight:195.261
Hs Code.:2933990090
European Community (EC) Number:810-959-4
DSSTox Substance ID:DTXSID101157679
Nikkaji Number:J989.579E
Mol file:188345-71-3.mol

Synonyms:702666-73-7;2-(tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene;tert-butyl (1R,4S)-2-azabicyclo[2.2.1]hept-5-ene-2-carboxylate;SCHEMBL12275013;ZATXHTCUZAWODK-BDAKNGLRSA-N;DTXSID101157679;AKOS016023721;AC-22987;tert-butyl 5-azabicyclo[2.2.1]hept-2-ene-5-carboxylate;(1R,4S)-tert-Butyl 2-azabicyclo[2.2.1]hept-5-ene-2-carboxylate;1,1-Dimethylethyl (1R,4S)-2-azabicyclo[2.2.1]hept-5-ene-2-carboxylate;(1R,4S)-2-Azabicyclo[2.2.1]hepta-5-ene-2-carboxylic acid tert-butyl ester

Suppliers and Price of 2-(Tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Boc-2-Azabicyclo[2.2.1]hept-5-ene
100mg
$ 60.00

TCI Chemical
2-(tert-Butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene >95.0%(GC)
1g
$ 94.00

Synthonix
2-Boc-2-Azabicyclo[2.2.1]hept-5-ene 95+%
10g
$ 660.00

Synthonix
2-Boc-2-Azabicyclo[2.2.1]hept-5-ene 95+%
25g
$ 1180.00

Matrix Scientific
2-Boc-2-Azabicyclo[2.2.1]hept-5-ene 95+%
1g
$ 1073.00

Crysdot
2-Boc-2-Azabicyclo[2.2.1]hept-5-ene 97%
10g
$ 238.00

Chem-Impex
2-(tert-Butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene,≥95%(GC) ≥95%(GC)
1G
$ 105.15

Chemenu
2-Boc-2-Azabicyclo[2.2.1]hept-5-ene 97%
10g
$ 284.00

Apolloscientific
2-Boc-2-azabicyclo[2.2.1]hept-5-ene 95%
1g
$ 280.00

Apolloscientific
2-Boc-2-azabicyclo[2.2.1]hept-5-ene 95%
250mg
$ 110.00

Total 40 raw suppliers

Chemical Property of 2-(Tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene

Chemical Property:

Vapor Pressure:0.013mmHg at 25°C
Refractive Index:1.4690-1.4730
Boiling Point:259.565oC at 760 mmHg
PKA:-0.88±0.20(Predicted)
Flash Point:110.781oC
PSA：29.54000
Density:1.105g/cm3
LogP:2.11970
Storage Temp.:2-8°C
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:195.125928785
Heavy Atom Count:14
Complexity:278

Purity/Quality:

99%, ^*data from raw suppliers

2-Boc-2-Azabicyclo[2.2.1]hept-5-ene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)N1CC2CC1C=C2
Isomeric SMILES:CC(C)(C)OC(=O)N1C[C@H]2C[C@@H]1C=C2

Technology Process of 2-(Tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene

There total 15 articles about 2-(Tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: (1S,4R,5R)-5-(Toluene-4-sulfonyl)-7-aza-bicyclo[2.2.1]hept-2-ene-7-carboxylic acid tert-butyl ester

: 188345-71-3
2-(tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene

: 192118-47-1
tert-butyl 7-azabicyclo[2.2.1]hept-2-ene-7-carboxylate

Guidance literature:: With sodium dihydrogenphosphate; sodium amalgam; In methanol; at -10 - 25 ℃; for 3h;
DOI:10.1039/b107414h

Reference yield: 45.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 24424-99-5
di-tert-butyl dicarbonate

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 188345-71-3
2-(tert-butoxycarbonyl)-2-azabicyclo[2.2.1]hept-5-ene

Guidance literature:: formaldehyd; cyclopenta-1,3-diene; With ammonium chloride; In water; at 20 ℃; for 17h;

di-tert-butyl dicarbonate; With sodium hydroxide; at 20 ℃; for 7h; pH=8; Further stages.;
DOI:10.1021/jm070018l