1-Bromo-6-methoxynaphthalen-2-ol

Base Information

Chemical Name:1-Bromo-6-methoxynaphthalen-2-ol
CAS No.:194594-62-2
Molecular Formula:C11H9BrO2
Molecular Weight:253.095
Hs Code.:
DSSTox Substance ID:DTXSID90593693
Wikidata:Q82488216
Mol file:194594-62-2.mol

Synonyms:1-bromo-6-methoxynaphthalen-2-ol;194594-62-2;2-HYDROXY-1-BROMO-6-METHOXY-NAPHTHALENE;SCHEMBL1359473;DTXSID90593693;BSHJGFUJGRDAAS-UHFFFAOYSA-N;1-bromo-6-methoxy-naphthalen-2-ol

Suppliers and Price of 1-Bromo-6-methoxynaphthalen-2-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-BROMO-6-METHOXYNAPHTHALEN-2-OL 95.00%
5G
$ 2367.75

American Custom Chemicals Corporation
1-BROMO-6-METHOXYNAPHTHALEN-2-OL 95.00%
1G
$ 981.75

Total 8 raw suppliers

Chemical Property of 1-Bromo-6-methoxynaphthalen-2-ol

Chemical Property:

PSA：29.46000
LogP:3.31650
XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:251.97859
Heavy Atom Count:14
Complexity:198

Purity/Quality:

99.3% ^*data from raw suppliers

1-BROMO-6-METHOXYNAPHTHALEN-2-OL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=C(C=C1)C(=C(C=C2)O)Br

Technology Process of 1-Bromo-6-methoxynaphthalen-2-ol

There total 4 articles about 1-Bromo-6-methoxynaphthalen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 5111-66-0
6-Methoxy-2-naphthol

: 194594-62-2
1-bromo-6-methoxynaphthalen-2-ol

Guidance literature:: With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 20 ℃; for 0.75h;
DOI:10.1021/jm050723z

Reference yield: 87.0%

: 128-08-5
N-Bromosuccinimide

: 5111-66-0
6-Methoxy-2-naphthol

: 194594-62-2
1-bromo-6-methoxynaphthalen-2-ol

Guidance literature:: In DMF (N,N-dimethyl-formamide); at 20 ℃; for 1.25h;

Reference yield:

: 581-43-1
2.6-dihydroxynaphthalene

: 194594-62-2
1-bromo-6-methoxynaphthalen-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 12 h / 20 °C

2.1: N-Bromosuccinimide / tetrachloromethane / 3 h / 0 - 20 °C

With N-Bromosuccinimide; potassium carbonate; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jacs.9b13117