Naphthalene, 1-(1-methylethoxy)- (9CI)

Base Information

• Chemical Name: Naphthalene, 1-(1-methylethoxy)- (9CI)
• CAS No.: 20009-27-2
• Molecular Formula: C13H14O
• Molecular Weight: 186.25000
• Mol file: 20009-27-2.mol

Synonyms:isopropyl-[1]naphthyl ether;1-isopropoxynaphthalene;1-Isopropyloxy-naphthalin;isopropyl-1-naphthylether;1-Isopentyloxy-naphthalin;Naphthalene, 1-(1-methylethoxy)-;Isopropyl-[1]naphthyl-aether;1-Isopropoxy-naphthalene;

Chemical Property of Naphthalene, 1-(1-methylethoxy)- (9CI)

Chemical Property:

• Melting Point: <-10 °C
• Boiling Point: 91 °C (0.4 mmHg)
• PSA: 9.23000
• Density: 1.029±0.06 g/cm3(Predicted)
• LogP: 3.62700

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Naphthalene, 1-(1-methylethoxy)- (9CI)

There total 8 articles about Naphthalene, 1-(1-methylethoxy)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

α-naphthol (90-15-3) + isopropyl bromide (75-26-3) → 1-isopropoxynaphthalene (20009-27-2)

Guidance literature:

With potassium carbonate; In neat (no solvent); at 125 ℃; for 2h; Microwave irradiation;

DOI:10.2174/1570178611310050005

Reference yield: 56.0%

isopropyl alcohol (67-63-0,8013-70-5) + 1-Chloronaphthalene (90-13-1) → 1-isopropoxynaphthalene (20009-27-2)

Guidance literature:

With C₃₄H₄₇ClNiO₃P₂; sodium t-butanolate; In toluene; at 110 ℃; for 18h; Inert atmosphere; Sealed tube;

DOI:10.1021/jacs.8b01800

Reference yield:

sodium naphtholate (3019-88-3) + isopropyl bromide (75-26-3) → 1-isopropoxynaphthalene (20009-27-2)

Guidance literature:

With 1,4-dioxane; potassium iodide;

DOI:10.1021/ja01186a006

upstream raw materials:

isopropyl chloride

sodium naphtholate

isopropyl bromide

1-Bromonaphthalene

Downstream raw materials:

2-Isopropoxy-1,8-diphenyl-1a,2,7,7a-tetrahydro-1,2,7-metheno-1H-cyclopropanaphthalin

1-(4-methylphenyl)naphthalene

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