Ethanamine, N-[(diphenylphosphino)methyl]-N-ethyl-

Base Information

Chemical Name:Ethanamine, N-[(diphenylphosphino)methyl]-N-ethyl-
CAS No.:2071-27-4
Molecular Formula:C17H22NP
Molecular Weight:271.342
Hs Code.:
DSSTox Substance ID:DTXSID90403682
Nikkaji Number:J810.680K
Wikidata:Q82207419

Synonyms:2071-27-4;N-((Diphenylphosphino)methyl)-N-ethylethanamine;Ethanamine, N-[(diphenylphosphino)methyl]-N-ethyl-;SCHEMBL8652282;DTXSID90403682

Suppliers and Price of Ethanamine, N-[(diphenylphosphino)methyl]-N-ethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Ethanamine, N-[(diphenylphosphino)methyl]-N-ethyl-

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:271.148986704
Heavy Atom Count:19
Complexity:209

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)CP(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of Ethanamine, N-[(diphenylphosphino)methyl]-N-ethyl-

There total 7 articles about Ethanamine, N-[(diphenylphosphino)methyl]-N-ethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 96776-80-6
diphenyl-bis(hydroxymethyl)phosphonium chloride

: 109-89-7
diethylamine

: 2071-27-4
<(diethylamino)methyl>diphenylphosphine

Guidance literature:: With triethylamine; In methanol; at 25 ℃; Inert atmosphere;
DOI:10.3390/ph15020169

Reference yield:

: 829-85-6
diphenylphosphane

: 2071-27-4
<(diethylamino)methyl>diphenylphosphine

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl ether / Inert atmosphere

1.2: Heating; Inert atmosphere

2.1: tetrahydrofuran-d8 / 1 h / Reflux; Inert atmosphere

In tetrahydrofuran-d8; diethyl ether;
DOI:10.1016/j.poly.2012.04.019

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 2071-27-4
<(diethylamino)methyl>diphenylphosphine

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; sodium carbonate / diethyl ether

2.1: lithium aluminium tetrahydride / diethyl ether

3.1: diethyl ether / Inert atmosphere

3.2: Heating; Inert atmosphere

4.1: tetrahydrofuran-d8 / 1 h / Reflux; Inert atmosphere

With lithium aluminium tetrahydride; water; sodium carbonate; In tetrahydrofuran-d8; diethyl ether;
DOI:10.1016/j.poly.2012.04.019