phenyl 4-methylbenzenecarbodithioate

Base Information

• Chemical Name: phenyl 4-methylbenzenecarbodithioate
• CAS No.: 20849-31-4
• Molecular Formula: C14H12S2
• Molecular Weight: 244.381
• Mol file: 20849-31-4.mol

Synonyms:p-Methyldithiobenzoesaeure-phenylester;phenyl 4-(methyl)dithiobenzoate;Phenyl 4-methyldithiobenzoate;p-Methyl-dithiobenzoesaeure-phenylester;

Chemical Property of phenyl 4-methylbenzenecarbodithioate

Chemical Property:

• PSA: 57.39000
• LogP: 4.46280

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl 4-methylbenzenecarbodithioate

There total 9 articles about phenyl 4-methylbenzenecarbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

S-phenyl 4-methylbenzothioate (3128-42-5) → 4-Methyldithiobenzoesaeurephenylester (20849-31-4)

Guidance literature:

With Lawessons reagent; In toluene; Heating;

Reference yield: 90.0%

4-(methyl)thiobenzoyl diphenylthiophosphinoyl sulfide (97270-52-5) → 4-Methyldithiobenzoesaeurephenylester (20849-31-4) + sodium 4-(methyl)dithiobenzoate (53724-36-0) + sodium diphenylphosphinodithioate (5827-17-8)

Guidance literature:

With sodium thiophenolate; In diethyl ether; at 16 - 22 ℃; for 4h;

Reference yield: 90.0%

bis(4-methylbenzenethiocarbonyl) sulphide (60410-77-7) + sodium thiophenolate (930-69-8) → 4-Methyldithiobenzoesaeurephenylester (20849-31-4)

Guidance literature:

In ethanol; hexane; for 3h; Ambient temperature;

upstream raw materials:

p-Methylthiobenzoyl-phenyl-disulfid

2-(4-methylphenyl)-1,3-dithiolane

2-carboxybenzene diazonium chloride

p-tolyl(phenylthio)sulfine

Downstream raw materials:

1-<4-(methyl)thiobenzoyl>piperidine

3-Phenyl-6-phenylsulfanyl-6-p-tolyl-4H-[1,5,2]oxathiazine

p-tolyl(phenylthio)sulfine

n-butyl p-tolyl ketone