1,6-DIMETHYL-4-(3-NITRO-PHENYL)-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER

Base Information

Chemical Name:1,6-DIMETHYL-4-(3-NITRO-PHENYL)-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER
CAS No.:219814-84-3
Molecular Formula:C15H17N3O5
Molecular Weight:319.317
Hs Code.:
Mol file:219814-84-3.mol

Synonyms:1,6-Dimethyl-4-(3-nitro-phenyl)-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester;Ethyl 1,6-dimethyl-4-(3-nitrophenyl)-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate;5-ethoxycarbonyl-1,6-dimethyl-4-(3-nitrophenyl)-3,4-dihydropyrimidin-2(1H)-one;

Suppliers and Price of 1,6-DIMETHYL-4-(3-NITRO-PHENYL)-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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American Custom Chemicals Corporation
1,6-DIMETHYL-4-(3-NITRO-PHENYL)-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER 95.00%
5MG
$ 503.65

Total 0 raw suppliers

Chemical Property of 1,6-DIMETHYL-4-(3-NITRO-PHENYL)-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER

Chemical Property:

Melting Point:136 - 137 °C (hexane)
PSA：104.46000
LogP:2.91790

Purity/Quality:: 1,6-DIMETHYL-4-(3-NITRO-PHENYL)-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

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Technology Process of 1,6-DIMETHYL-4-(3-NITRO-PHENYL)-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER

There total 3 articles about 1,6-DIMETHYL-4-(3-NITRO-PHENYL)-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 123371-44-8,110448-29-8
nifetepimine

: 74-88-4
methyl iodide

: 219814-84-3
1,6-dimethyl-4-(3-nitro-phenyl)-2-oxo-1,2,3,4-tetrahydro-pyrimidine-5-carboxylic acid ethyl ester

Guidance literature:: nifetepimine; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 17h; regioselective reaction;
DOI:10.1016/j.ejmech.2012.04.043