Cyclopropaneacetic acid, a-acetyl-, ethyl ester

Base Information

Chemical Name:Cyclopropaneacetic acid, a-acetyl-, ethyl ester
CAS No.:22396-14-1
Molecular Formula:C9H14O3
Molecular Weight:170.20600
Hs Code.:
Mol file:22396-14-1.mol

Synonyms:ethyl 2-cyclopropyl-3-oxobutanoate;2-Cyclopropyl-3-oxo-butyric acid ethyl ester;

Suppliers and Price of Cyclopropaneacetic acid, a-acetyl-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
ethyl2-cyclopropyl-3-oxobutanoate
250mg
$ 350.00

TRC
ethyl2-cyclopropyl-3-oxobutanoate
50mg
$ 90.00

Total 1 raw suppliers

Chemical Property of Cyclopropaneacetic acid, a-acetyl-, ethyl ester

Chemical Property:

PSA：43.37000
LogP:1.16470

Purity/Quality:: ethyl2-cyclopropyl-3-oxobutanoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclopropaneacetic acid, a-acetyl-, ethyl ester

There total 2 articles about Cyclopropaneacetic acid, a-acetyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 918907-28-5
2-cyclopropyl-3-oxobutyronitrile

: 64-17-5
ethanol

: 22396-14-1
2-cyclopropyl-3-oxobutyric acid ethyl ester

Guidance literature:: 2-cyclopropyl-3-oxobutyronitrile; With ethanol; acetyl chloride; at 20 ℃;

ethanol; With hydrogenchloride; In tetrahydrofuran; at 40 ℃; for 2h;
DOI:10.1016/j.bmcl.2006.09.005

Reference yield:

: 6542-60-5
2-cyclopropylacetonitrile

: 22396-14-1
2-cyclopropyl-3-oxobutyric acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium N,N-diisopropylamide / cyclohexane; tetrahydrofuran / 0.17 h / cooling

1.2: 78 percent / tetrahydrofuran; cyclohexane / 0.17 h / 20 °C

2.1: acetyl chloride; EtOH / 20 °C

2.2: 89 percent / aq. HCl / tetrahydrofuran / 2 h / 40 °C

With ethanol; acetyl chloride; lithium diisopropyl amide; In tetrahydrofuran; cyclohexane;
DOI:10.1016/j.bmcl.2006.09.005