2,6-dichloro-4-nitrobenzoic acid

Base Information

Chemical Name:2,6-dichloro-4-nitrobenzoic acid
CAS No.:22509-50-8
Molecular Formula:C7H3Cl2NO4
Molecular Weight:236.011
Hs Code.:2916399090
Mol file:22509-50-8.mol

Synonyms:2.6-Dichlor-4-nitro-benzoesaeure;2,6-dichloro-4-nitro-benzoic acid;

Suppliers and Price of 2,6-dichloro-4-nitrobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,6-DICHLORO-4-NITROBENZOIC ACID 95.00%
5MG
$ 497.76

Alichem
2,6-Dichloro-4-nitrobenzoicacid
1g
$ 1445.30

Alichem
2,6-Dichloro-4-nitrobenzoicacid
250mg
$ 480.00

Total 8 raw suppliers

Chemical Property of 2,6-dichloro-4-nitrobenzoic acid

Chemical Property:

Melting Point:175.6-176.4 °C(Solv: water (7732-18-5))
Boiling Point:366.3±42.0 °C(Predicted)
PKA:0.85±0.26(Predicted)
PSA：83.12000
Density:1.713±0.06 g/cm3(Predicted)
LogP:3.12300

Purity/Quality:

98%Min ^*data from raw suppliers

2,6-DICHLORO-4-NITROBENZOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,6-dichloro-4-nitrobenzoic acid

There total 2 articles about 2,6-dichloro-4-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 7149-69-1
1,3-dichloro-2-methyl-5-nitrobenzene

: 22509-50-8
2,6-dichloro-4-nitrobenzoic acid

Guidance literature:: With potassium permanganate; In pyridine; water; for 28h; Reflux;
DOI:10.1016/j.tet.2015.12.026

Reference yield:

: 99-99-0
1-methyl-4-nitrobenzene

: 22509-50-8
2,6-dichloro-4-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: chlorine; antimony(III) chloride / 65 °C

2: potassium permanganate / water; pyridine / Reflux

With potassium permanganate; antimony(III) chloride; chlorine; In pyridine; water;
DOI:10.1016/j.bmc.2015.08.021

Reference yield: 84.0%

: 67-56-1
methanol

: 22509-50-8
2,6-dichloro-4-nitrobenzoic acid

: 232275-50-2
methyl 2,6-dichloro-4-nitrobenzoate

Guidance literature:: 2,6-dichloro-4-nitrobenzoic acid; With thionyl chloride; N,N-dimethyl-formamide; In 1,2-dichloro-ethane; for 2h; Reflux;

methanol; at 50 ℃; for 20h;
DOI:10.1016/j.tet.2015.12.026